n-pent-4-yl 2,3,4-O-tribenzyl-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

Base Information

Chemical Name:n-pent-4-yl 2,3,4-O-tribenzyl-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside
CAS No.:127570-60-9
Molecular Formula:C₄₈H₅₆O₆Si
Molecular Weight:757.055
Hs Code.:

Synonyms:n-pent-4-yl 2,3,4-O-tribenzyl-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

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Chemical Property of n-pent-4-yl 2,3,4-O-tribenzyl-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

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Technology Process of n-pent-4-yl 2,3,4-O-tribenzyl-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

There total 3 articles about n-pent-4-yl 2,3,4-O-tribenzyl-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 127570-63-2
C₂₇H₃₈O₆Si

: 100-39-0
benzyl bromide

: 127570-60-9
n-pent-4-yl 2,3,4-O-tribenzyl-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201001278

Reference yield:

: 50256-33-2
n-pent-4-enyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

: 127570-60-9
n-pent-4-yl 2,3,4-O-tribenzyl-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: methanol; sodium methylate / tetrahydrofuran / 4 h

2: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C

3: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; methanol; sodium methylate; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201001278

Reference yield:

: 125631-33-6
4-penten-1-yl-β-D-glucopyranoside

: 127570-60-9
n-pent-4-yl 2,3,4-O-tribenzyl-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C

2: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201001278