2-{[1-(1,1-dimethylethyl)-3-phenylprop-2-yn-1-yl]oxy}-N-methyl-N-methoxyacetamide

Base Information

Chemical Name:2-{[1-(1,1-dimethylethyl)-3-phenylprop-2-yn-1-yl]oxy}-N-methyl-N-methoxyacetamide
CAS No.:923026-38-4
Molecular Formula:C₁₇H₂₃NO₃
Molecular Weight:289.375
Hs Code.:

Synonyms:2-{[1-(1,1-dimethylethyl)-3-phenylprop-2-yn-1-yl]oxy}-N-methyl-N-methoxyacetamide

Suppliers and Price of 2-{[1-(1,1-dimethylethyl)-3-phenylprop-2-yn-1-yl]oxy}-N-methyl-N-methoxyacetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-{[1-(1,1-dimethylethyl)-3-phenylprop-2-yn-1-yl]oxy}-N-methyl-N-methoxyacetamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-{[1-(1,1-dimethylethyl)-3-phenylprop-2-yn-1-yl]oxy}-N-methyl-N-methoxyacetamide

There total 2 articles about 2-{[1-(1,1-dimethylethyl)-3-phenylprop-2-yn-1-yl]oxy}-N-methyl-N-methoxyacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 923026-34-0
{[1-(1,1-dimethylethyl)-3-phenylprop-2-yn-1-yl]oxy}acetic acid

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 923026-38-4
2-{[1-(1,1-dimethylethyl)-3-phenylprop-2-yn-1-yl]oxy}-N-methyl-N-methoxyacetamide

Guidance literature:: {[1-(1,1-dimethylethyl)-3-phenylprop-2-yn-1-yl]oxy}acetic acid; With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; In dichloromethane; for 0.5h;

N,O-dimethylhydroxylamine*hydrochloride; With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 2h;
DOI:10.1002/hlca.200690241

Reference yield:

: 132350-97-1,29586-01-4
4,4-dimethyl-1-phenyl-pent-1-yn-3-ol

: 923026-38-4
2-{[1-(1,1-dimethylethyl)-3-phenylprop-2-yn-1-yl]oxy}-N-methyl-N-methoxyacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: TBTU; (i-Pr)2NEt

With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine;
DOI:10.1055/s-2006-958949

Reference yield: 82.0%

: 923026-38-4
2-{[1-(1,1-dimethylethyl)-3-phenylprop-2-yn-1-yl]oxy}-N-methyl-N-methoxyacetamide

: 536-74-3
phenylacetylene

: 923026-56-6
1-{[1-(1,1-dimethylethyl)-3-phenylprop-2-yn-1-yl]oxy}-4-phenylbut-3-yn-2-one

Guidance literature:: phenylacetylene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h;

2-{[1-(1,1-dimethylethyl)-3-phenylprop-2-yn-1-yl]oxy}-N-methyl-N-methoxyacetamide; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1002/hlca.200690241