7-(1-phenyl-1H-tetrazole-5-ylthio)heptyl pivalate

Base Information

Chemical Name:7-(1-phenyl-1H-tetrazole-5-ylthio)heptyl pivalate
CAS No.:1446326-25-5
Molecular Formula:C₁₉H₂₈N₄O₂S
Molecular Weight:376.523
Hs Code.:

Synonyms:7-(1-phenyl-1H-tetrazole-5-ylthio)heptyl pivalate

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Chemical Property of 7-(1-phenyl-1H-tetrazole-5-ylthio)heptyl pivalate

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Technology Process of 7-(1-phenyl-1H-tetrazole-5-ylthio)heptyl pivalate

There total 1 articles about 7-(1-phenyl-1H-tetrazole-5-ylthio)heptyl pivalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1446326-24-4
7-bromoheptyl pivalate

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 1446326-25-5
7-(1-phenyl-1H-tetrazole-5-ylthio)heptyl pivalate

Guidance literature:: With potassium carbonate; In acetone; Reflux;
DOI:10.1016/j.tet.2013.04.134

Reference yield: 86.0%

: 1446326-25-5
7-(1-phenyl-1H-tetrazole-5-ylthio)heptyl pivalate

: 1411491-41-2
2,2-dimethylpropionic acid-7-(1-phenyl-1H-tetrazol-5-ylsulfonyl)-heptyl ester

Guidance literature:: With ammonium molybdate tetrahydrate; dihydrogen peroxide; at 15 - 20 ℃; for 18.67h;
DOI:10.1016/j.tet.2013.04.134

Reference yield:

: 1446326-25-5
7-(1-phenyl-1H-tetrazole-5-ylthio)heptyl pivalate

: methyl 2-((1R,2R)-1-(tert-butyldimethylsilyloxy)-10-(1-phenyl-1H-tetrazol-5-ylthio)decyl)hexacosanoate

Guidance literature:: Multi-step reaction with 6 steps

1: dihydrogen peroxide; ammonium molybdate tetrahydrate / 18.67 h / 15 - 20 °C

2: lithium hexamethyldisilazane / tetrahydrofuran / 18 h / 20 °C

3: hydrogen; palladium 10% on activated carbon / tetrahydrofuran; ethanol / 18 h / 20 °C / 760.05 Torr

4: potassium hydroxide / tetrahydrofuran; methanol; water / 2 h / 70 °C / Reflux

5: sodium hydrogencarbonate; N-Bromosuccinimide; triphenylphosphine / dichloromethane / 1.17 h / 0 - 4 °C

6: potassium carbonate / tetrahydrofuran; acetone / 18 h / 20 °C

With N-Bromosuccinimide; ammonium molybdate tetrahydrate; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; sodium hydrogencarbonate; potassium carbonate; triphenylphosphine; potassium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetone; 2: |Julia-Kocienski Olefination;
DOI:10.1016/j.tet.2013.04.134