2,2-dimethylpropionic acid-7-(1-phenyl-1H-tetrazol-5-ylsulfonyl)-heptyl ester

Base Information

Chemical Name:2,2-dimethylpropionic acid-7-(1-phenyl-1H-tetrazol-5-ylsulfonyl)-heptyl ester
CAS No.:1411491-41-2
Molecular Formula:C₁₉H₂₈N₄O₄S
Molecular Weight:408.522
Hs Code.:

Synonyms:2,2-dimethylpropionic acid-7-(1-phenyl-1H-tetrazol-5-ylsulfonyl)-heptyl ester

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Chemical Property of 2,2-dimethylpropionic acid-7-(1-phenyl-1H-tetrazol-5-ylsulfonyl)-heptyl ester

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Technology Process of 2,2-dimethylpropionic acid-7-(1-phenyl-1H-tetrazol-5-ylsulfonyl)-heptyl ester

There total 1 articles about 2,2-dimethylpropionic acid-7-(1-phenyl-1H-tetrazol-5-ylsulfonyl)-heptyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1446326-25-5
7-(1-phenyl-1H-tetrazole-5-ylthio)heptyl pivalate

: 1411491-41-2
2,2-dimethylpropionic acid-7-(1-phenyl-1H-tetrazol-5-ylsulfonyl)-heptyl ester

Guidance literature:: With ammonium molybdate tetrahydrate; dihydrogen peroxide; at 15 - 20 ℃; for 18.67h;
DOI:10.1016/j.tet.2013.04.134

Reference yield: 69.0%

: 918905-62-1
trans-(1S,2R)-2-[(S)-3-(tert-butyldiphenylsilanyloxy)-1-methylpropyl]cyclopropanecarbaldehyde

: 1411491-41-2
2,2-dimethylpropionic acid-7-(1-phenyl-1H-tetrazol-5-ylsulfonyl)-heptyl ester

: 2,2-dimethylpropionic acid 8-{(1R,2R)-2-[(S)-3-(tert-butyldiphenylsilanyloxy)-1-methyl-propyl]cyclopropyl}oct-7-enyl ester

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at -12 - 20 ℃; for 20h;
DOI:10.1016/j.tet.2013.04.134

Reference yield:

: 1411491-41-2
2,2-dimethylpropionic acid-7-(1-phenyl-1H-tetrazol-5-ylsulfonyl)-heptyl ester

: 1411489-71-8
5-((15S,16S)-15-methoxy-16-methyltetratriacontyl-1-sulfonyl)-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 6 steps

1: lithium hexamethyldisilazane / tetrahydrofuran / 18 h / -12 - -5 °C / Inert atmosphere

2: hydrogen; palladium 10% on activated carbon / tetrahydrofuran / 760.05 Torr

3: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / -20 °C / Inert atmosphere; Reflux

4: N-Bromosuccinimide; triphenylphosphine / dichloromethane; ethanol / 1 h / 0 - 20 °C

5: potassium carbonate / tetrahydrofuran; acetone / 18 h / 20 °C

6: 3-chloro-benzenecarboperoxoic acid; sodium hydrogencarbonate / dichloromethane / 18 h / 20 °C

With N-Bromosuccinimide; lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; lithium hexamethyldisilazane; In tetrahydrofuran; ethanol; dichloromethane; acetone; 1: |Julia-Kocienski Olefination;
DOI:10.1016/j.tet.2013.04.134