9-(2-hydroxy-ethyl)-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid benzyl-methyl-amide

Base Information

Chemical Name:9-(2-hydroxy-ethyl)-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid benzyl-methyl-amide
CAS No.:1246453-84-8
Molecular Formula:C₂₃H₂₆N₂O₂
Molecular Weight:362.472
Hs Code.:

Synonyms:9-(2-hydroxy-ethyl)-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid benzyl-methyl-amide

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Chemical Property of 9-(2-hydroxy-ethyl)-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid benzyl-methyl-amide

Chemical Property:

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Technology Process of 9-(2-hydroxy-ethyl)-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid benzyl-methyl-amide

There total 7 articles about 9-(2-hydroxy-ethyl)-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid benzyl-methyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1246453-83-7
9-(2-benzyloxy-ethyl)-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid benzyl-methyl-amide

: 1246453-84-8
9-(2-hydroxy-ethyl)-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid benzyl-methyl-amide

Guidance literature:: In methanol;

Reference yield:

: 1246453-82-6
9-(2-benzyloxy-ethyl)-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid

: 1246453-84-8
9-(2-hydroxy-ethyl)-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid benzyl-methyl-amide

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride / dichloromethane

2: dichloromethane

3: palladium on activated charcoal; hydrogen / methanol

With oxalyl dichloride; palladium on activated charcoal; hydrogen; In methanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.12.084

Reference yield:

: 1246453-81-5
9-(2-benzyloxy-ethyl)-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid ethyl ester

: 1246453-84-8
9-(2-hydroxy-ethyl)-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid benzyl-methyl-amide

Guidance literature:: Multi-step reaction with 4 steps

1: water; sodium hydroxide / ethanol

2: oxalyl dichloride / dichloromethane

3: dichloromethane

4: palladium on activated charcoal; hydrogen / methanol

With oxalyl dichloride; palladium on activated charcoal; water; hydrogen; sodium hydroxide; In methanol; ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.12.084