methanesulfonic acid 2-[4-(benzyl-methyl-carbamoyl)-1,2,3,4-tetrahydro-carbazol-9-yl]-ethyl ester

Base Information

Chemical Name:methanesulfonic acid 2-[4-(benzyl-methyl-carbamoyl)-1,2,3,4-tetrahydro-carbazol-9-yl]-ethyl ester
CAS No.:1246453-85-9
Molecular Formula:C₂₄H₂₈N₂O₄S
Molecular Weight:440.563
Hs Code.:

Synonyms:methanesulfonic acid 2-[4-(benzyl-methyl-carbamoyl)-1,2,3,4-tetrahydro-carbazol-9-yl]-ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methanesulfonic acid 2-[4-(benzyl-methyl-carbamoyl)-1,2,3,4-tetrahydro-carbazol-9-yl]-ethyl ester

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Technology Process of methanesulfonic acid 2-[4-(benzyl-methyl-carbamoyl)-1,2,3,4-tetrahydro-carbazol-9-yl]-ethyl ester

There total 7 articles about methanesulfonic acid 2-[4-(benzyl-methyl-carbamoyl)-1,2,3,4-tetrahydro-carbazol-9-yl]-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 1246453-84-8
9-(2-hydroxy-ethyl)-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid benzyl-methyl-amide

: 124-63-0
methanesulfonyl chloride

: 1246453-85-9
methanesulfonic acid 2-[4-(benzyl-methyl-carbamoyl)-1,2,3,4-tetrahydro-carbazol-9-yl]-ethyl ester

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 1246453-82-6
9-(2-benzyloxy-ethyl)-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid

: 1246453-85-9
methanesulfonic acid 2-[4-(benzyl-methyl-carbamoyl)-1,2,3,4-tetrahydro-carbazol-9-yl]-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl dichloride / dichloromethane

2: dichloromethane

3: palladium on activated charcoal; hydrogen / methanol

4: dichloromethane

With oxalyl dichloride; palladium on activated charcoal; hydrogen; In methanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.12.084

Reference yield:

: 1246453-83-7
9-(2-benzyloxy-ethyl)-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid benzyl-methyl-amide

: 1246453-85-9
methanesulfonic acid 2-[4-(benzyl-methyl-carbamoyl)-1,2,3,4-tetrahydro-carbazol-9-yl]-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: palladium on activated charcoal; hydrogen / methanol

2: dichloromethane

With palladium on activated charcoal; hydrogen; In methanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.12.084