Technology Process of 5,6-dimethoxy-1,3-diphenyl-1H-indene
There total 9 articles about 5,6-dimethoxy-1,3-diphenyl-1H-indene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bismuth(lll) trifluoromethanesulfonate;
In
dichloromethane;
at 20 ℃;
for 1h;
DOI:10.1016/j.tet.2017.05.006
- Guidance literature:
-
Multi-step reaction with 3 steps
1: boron trifluoride diethyl etherate / dichloromethane / 20 h / 20 °C
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 20 °C
3: bismuth(lll) trifluoromethanesulfonate / dichloromethane / 1 h / 20 °C
With
bismuth(lll) trifluoromethanesulfonate; boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
1: |Friedel-Crafts Alkylation;
DOI:10.1016/j.tet.2017.05.006
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydroxide / methanol / Reflux
2: sodium tetrahydroborate / tetrahydrofuran; methanol / 0.5 h / 20 °C
3: boron trifluoride diethyl etherate / dichloromethane / 20 h / 20 °C
4: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 20 °C
5: bismuth(lll) trifluoromethanesulfonate / dichloromethane / 1 h / 20 °C
With
bismuth(lll) trifluoromethanesulfonate; sodium tetrahydroborate; boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane;
1: |Aldol Condensation / 3: |Friedel-Crafts Alkylation;
DOI:10.1016/j.tet.2017.05.006
