dimethyl α-aminobenzylphosphonate hydrochloride

Base Information

• Chemical Name: dimethyl α-aminobenzylphosphonate hydrochloride
• CAS No.: 70858-88-7
• Molecular Formula: C₉H₁₄NO₃P*ClH
• Molecular Weight: 251.65
• Mol file: 70858-88-7.mol

Synonyms:dimethyl α-aminobenzylphosphonate hydrochloride

Chemical Property of dimethyl α-aminobenzylphosphonate hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dimethyl α-aminobenzylphosphonate hydrochloride

There total 1 articles about dimethyl α-aminobenzylphosphonate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.4%

benzaldehyde (100-52-7) + Dimethyl phosphite (868-85-9) → dimethyl α-aminobenzylphosphonate hydrochloride (70858-88-7)

Guidance literature:

benzaldehyde; Dimethyl phosphite; With ammonium acetate; 4 A molecular sieve; In ethanol; at 60 ℃; for 44h;

With hydrogenchloride; In diethyl ether; ethanol;

DOI:10.1002/hc.20227

Reference yield: 76.5%

pyridine-4-carboxylic acid (55-22-1) + dimethyl α-aminobenzylphosphonate hydrochloride (70858-88-7) → dimethyl phenyl(4-pyridylcarbonylamino)methylphosphonate

Guidance literature:

With hexachloroethane; triethylamine; triphenylphosphine; In 1,2-dichloro-ethane; at 0 ℃; for 24h;

DOI:10.1002/hc.20227

upstream raw materials:

benzaldehyde

Dimethyl phosphite