(+/-)-methyl α-<2-ethyl>-2-chlorobenzeneacetate

Base Information

Chemical Name:(+/-)-methyl α-<2-ethyl>-2-chlorobenzeneacetate
CAS No.:116078-69-4
Molecular Formula:C₁₇H₂₆ClNO₂
Molecular Weight:311.852
Hs Code.:

(+/-)-methyl α-<2-<bis(1-methylethyl)amino>ethyl>-2-chlorobenzeneacetate

Synonyms:(+/-)-methyl α-<2-ethyl>-2-chlorobenzeneacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-methyl α-<2-ethyl>-2-chlorobenzeneacetate

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Technology Process of (+/-)-methyl α-<2-ethyl>-2-chlorobenzeneacetate

There total 2 articles about (+/-)-methyl α-<2-ethyl>-2-chlorobenzeneacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 67-56-1
methanol

: 68284-62-8
(+/-)-α-<2-ethyl>-2-chlorophenylacetonitrile

: 116078-69-4
(+/-)-methyl α-<2-ethyl>-2-chlorobenzeneacetate

Guidance literature:: With sulfuric acid; for 6h; Heating;
DOI:10.1021/jm00119a017

Reference yield:

: 68284-62-8
(+/-)-α-<2-ethyl>-2-chlorophenylacetonitrile

: 116078-69-4
(+/-)-methyl α-<2-ethyl>-2-chlorobenzeneacetate

Guidance literature:: With sulfuric acid; In methanol;

Reference yield: 37.0%

: 1440-60-4
1-chloroacetyl-piperidine

: 116078-69-4
(+/-)-methyl α-<2-ethyl>-2-chlorobenzeneacetate

: 116078-72-9
(+/-)-methyl α-<2-ethyl>-α-(2-chlorophenyl)-γ-oxo-1-piperidinebutanoate

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; 1.) 0 deg C, 30 min, 2.) -50 deg C, 30 min, room temperature, 2 h;
DOI:10.1021/jm00119a017