C₅₆H₇₃NO₁₄Si

Base Information

Chemical Name:C₅₆H₇₃NO₁₄Si
CAS No.:350583-43-6
Molecular Formula:C₅₆H₇₃NO₁₄Si
Molecular Weight:1012.28
Hs Code.:

C<sub>56</sub>H<sub>73</sub>NO<sub>14</sub>Si

Synonyms:C₅₆H₇₃NO₁₄Si

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Chemical Property of C₅₆H₇₃NO₁₄Si

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Technology Process of C₅₆H₇₃NO₁₄Si

There total 16 articles about C₅₆H₇₃NO₁₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 149249-91-2
(3R,4S)-1-benzoyl-4-phenyl-3-(triethylsilyl)oxy-2-azetidinone

: 350583-33-4
C₃₄H₄₆O₁₁

: 350583-43-6
C₅₆H₇₃NO₁₄Si

Guidance literature:: With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 3h;
DOI:10.1002/1099-0690(200105)2001:9<1761::AID-EJOC1761>3.0.CO;2-O

Reference yield:

: 350583-27-6
1,2-benzylidene-9,10-isopropylidene-5α-acetyltaxicin-I

: 350583-43-6
C₅₆H₇₃NO₁₄Si

Guidance literature:: Multi-step reaction with 9 steps

1: PBu₃; NEt₃; HCOOH / Pd(dba)2 / tetrahydrofuran / Heating

2: 67 percent / OsO₄; NMMO / tetrahydrofuran; H₂O; 2-methyl-propan-2-ol / 144 h / 20 °C

3: 61 percent / DIBALH / CH₂Cl₂; toluene / 0.5 h

4: 70 percent / pyridine / 4 °C

5: 79 percent / imidazole / dimethylformamide / 20 °C

6: 39 percent / lithium bis(trimethylsilyl)amide / tetrahydrofuran / -78 °C

7: 43 percent / tert-butyl hydroperoxide; palladium(II) acetate / toluene / 24 h / 60 °C

8: 73 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.17 h / 20 °C

9: 70 percent / sodium bis(trimethylsilyl)amide / tetrahydrofuran / 3 h / -78 °C

With 1H-imidazole; tert.-butylhydroperoxide; osmium(VIII) oxide; formic acid; tributylphosphine; tetrabutyl ammonium fluoride; palladium diacetate; sodium hexamethyldisilazane; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; triethylamine; lithium hexamethyldisilazane; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; pyridine; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;
DOI:10.1002/1099-0690(200105)2001:9<1761::AID-EJOC1761>3.0.CO;2-O

Reference yield:

: 994-30-9
triethylsilyl chloride

: 350583-43-6
C₅₆H₇₃NO₁₄Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: 96 percent / triethylamine / tetrahydrofuran

2.1: 2.58 g / H₂ / Pd/C / ethyl acetate / 20 h

3.1: trimethylsilyl chloride / diethyl ether / 1 h / 20 °C

3.2: 62 percent / tert-butylmagnesium chloride / diethyl ether / 3 h / 20 °C

4.1: 87 percent / triethylamine; 4-(dimethylamino)pyridine / CH₂Cl₂ / 20 h / 20 °C

5.1: 70 percent / sodium bis(trimethylsilyl)amide / tetrahydrofuran / 3 h / -78 °C

With dmap; chloro-trimethyl-silane; hydrogen; sodium hexamethyldisilazane; triethylamine; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1002/1099-0690(200105)2001:9<1761::AID-EJOC1761>3.0.CO;2-O