2,4-dichloro-5-fluorobenzoylacetic acid

Base Information

Chemical Name:2,4-dichloro-5-fluorobenzoylacetic acid
CAS No.:111760-50-0
Molecular Formula:C₉H₅Cl₂FO₃
Molecular Weight:251.041
Hs Code.:

Synonyms:2,4-dichloro-5-fluorobenzoylacetic acid

Suppliers and Price of 2,4-dichloro-5-fluorobenzoylacetic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,4-dichloro-5-fluorobenzoylacetic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,4-dichloro-5-fluorobenzoylacetic acid

There total 1 articles about 2,4-dichloro-5-fluorobenzoylacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 704-10-9
2,4-dichloro-5-fluoroacetophenone

: methyl magnesium carbonate

: 111760-50-0
2,4-dichloro-5-fluorobenzoylacetic acid

Guidance literature:: In N,N-dimethyl-formamide; at 110 ℃; for 1h; Yield given;

Reference yield:

: 111760-50-0
2,4-dichloro-5-fluorobenzoylacetic acid

: 122-51-0
orthoformic acid triethyl ester

: 371-40-4
4-fluoroaniline

: (Z)-2,4-dichloro-5-fluoro-α-[[(4-fluorophenyl)amino]methylene]-β-oxobenzenepropanoic acid, ethyl ester

Guidance literature:: With acetic anhydride; In ethanol; hexane;

Reference yield:

: 111760-50-0
2,4-dichloro-5-fluorobenzoylacetic acid

: 129527-47-5
methyl-2,4-dichloro-5-fluoro-α-(4-fluoro-2-methylphenylhydrazono)benzoylacetate

Guidance literature:: Multi-step reaction with 2 steps

1: HCl(gas) / methanol / 20 h / Ambient temperature

2: 1.) NaNO₂, aq. HCl, 2.) potassium acetate / 1.) 0 deg C, 30 min, 2.) water, methanol, dioxane, a) 5 deg C, 30 min, b) RT, 2 h

With hydrogenchloride; potassium acetate; sodium nitrite; In methanol;