methyl-2,4-dichloro-5-fluoro-α-(4-fluoro-2-methylphenylhydrazono)benzoylacetate

Base Information

Chemical Name:methyl-2,4-dichloro-5-fluoro-α-(4-fluoro-2-methylphenylhydrazono)benzoylacetate
CAS No.:129527-47-5
Molecular Formula:C₁₇H₁₂Cl₂F₂N₂O₃
Molecular Weight:401.197
Hs Code.:

Synonyms:methyl-2,4-dichloro-5-fluoro-α-(4-fluoro-2-methylphenylhydrazono)benzoylacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl-2,4-dichloro-5-fluoro-α-(4-fluoro-2-methylphenylhydrazono)benzoylacetate

Chemical Property:

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Technology Process of methyl-2,4-dichloro-5-fluoro-α-(4-fluoro-2-methylphenylhydrazono)benzoylacetate

There total 3 articles about methyl-2,4-dichloro-5-fluoro-α-(4-fluoro-2-methylphenylhydrazono)benzoylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 704-10-9
2,4-dichloro-5-fluoroacetophenone

: 129527-47-5
methyl-2,4-dichloro-5-fluoro-α-(4-fluoro-2-methylphenylhydrazono)benzoylacetate

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylformamide / 1 h / 110 °C

2: HCl(gas) / methanol / 20 h / Ambient temperature

3: 1.) NaNO₂, aq. HCl, 2.) potassium acetate / 1.) 0 deg C, 30 min, 2.) water, methanol, dioxane, a) 5 deg C, 30 min, b) RT, 2 h

With hydrogenchloride; potassium acetate; sodium nitrite; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 111760-50-0
2,4-dichloro-5-fluorobenzoylacetic acid

: 129527-47-5
methyl-2,4-dichloro-5-fluoro-α-(4-fluoro-2-methylphenylhydrazono)benzoylacetate

Guidance literature:: Multi-step reaction with 2 steps

1: HCl(gas) / methanol / 20 h / Ambient temperature

2: 1.) NaNO₂, aq. HCl, 2.) potassium acetate / 1.) 0 deg C, 30 min, 2.) water, methanol, dioxane, a) 5 deg C, 30 min, b) RT, 2 h

With hydrogenchloride; potassium acetate; sodium nitrite; In methanol;

Reference yield:

: 452-71-1
4-fluor-2-methylaniline

: 103319-17-1
methyl 2,4-dichloro-5-fluoro-benzoylacetate

: 129527-47-5
methyl-2,4-dichloro-5-fluoro-α-(4-fluoro-2-methylphenylhydrazono)benzoylacetate

Guidance literature:: With hydrogenchloride; potassium acetate; sodium nitrite; Yield given. Multistep reaction; 1.) 0 deg C, 30 min, 2.) water, methanol, dioxane, a) 5 deg C, 30 min, b) RT, 2 h;