(+/-)-1-(3-chlorophenyl)-1-[4-(pyrrolidin-1-ylmethyl)phenyl]methylamine

Base Information

Chemical Name:(+/-)-1-(3-chlorophenyl)-1-[4-(pyrrolidin-1-ylmethyl)phenyl]methylamine
CAS No.:1050527-75-7
Molecular Formula:C₁₈H₂₁ClN₂
Molecular Weight:300.831
Hs Code.:

Synonyms:(+/-)-1-(3-chlorophenyl)-1-[4-(pyrrolidin-1-ylmethyl)phenyl]methylamine

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Chemical Property of (+/-)-1-(3-chlorophenyl)-1-[4-(pyrrolidin-1-ylmethyl)phenyl]methylamine

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Technology Process of (+/-)-1-(3-chlorophenyl)-1-[4-(pyrrolidin-1-ylmethyl)phenyl]methylamine

There total 2 articles about (+/-)-1-(3-chlorophenyl)-1-[4-(pyrrolidin-1-ylmethyl)phenyl]methylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 898776-32-4
(3-chlorophenyl)[4-(pyrrolidin-1-ylmethyl)phenyl]methanone

: 1050527-75-7
(+/-)-1-(3-chlorophenyl)-1-[4-(pyrrolidin-1-ylmethyl)phenyl]methylamine

Guidance literature:: (3-chlorophenyl)[4-(pyrrolidin-1-ylmethyl)phenyl]methanone; With titanium(IV) isopropylate; ammonia; In ethanol; for 16h;

With sodium tetrahydroborate; In ethanol; at 20 ℃; for 3h;

Reference yield:

: 945657-22-7
(4-bromomethyl-phenyl)(3-chloro-phenyl)methanone

: 1050527-75-7
(+/-)-1-(3-chlorophenyl)-1-[4-(pyrrolidin-1-ylmethyl)phenyl]methylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / acetonitrile / 1 h / 0 °C

2.1: titanium(IV) isopropylate; ammonia / ethanol / 16 h

2.2: 3 h / 20 °C

With titanium(IV) isopropylate; ammonia; triethylamine; In ethanol; acetonitrile;

Reference yield: 70.0%

: 86-98-6,1138471-54-1
4,7-dichloroquinoline

: 1050527-75-7
(+/-)-1-(3-chlorophenyl)-1-[4-(pyrrolidin-1-ylmethyl)phenyl]methylamine

: 1050526-88-9
(+/-)-7-chloro-N-{(3-chlorophenyl)[4-(pyrrolidin-1-ylmethyl)phenyl]methyl}-4-aminoquinoline

Guidance literature:: 4,7-dichloroquinoline; (+/-)-1-(3-chlorophenyl)-1-[4-(pyrrolidin-1-ylmethyl)phenyl]methylamine; With pyridine hydrochloride; In 2-ethoxy-ethanol; at 135 ℃; for 5h;

With triethylamine; In 2-ethoxy-ethanol; at 20 ℃;