methyl 2,3-di-O-benzyl-6-chloroacetamido-6-deoxy-4-O-methyl-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2,3-di-O-benzyl-6-chloroacetamido-6-deoxy-4-O-methyl-α-D-glucopyranoside
CAS No.:193287-50-2
Molecular Formula:C₂₄H₃₀ClNO₆
Molecular Weight:463.958
Hs Code.:

Synonyms:methyl 2,3-di-O-benzyl-6-chloroacetamido-6-deoxy-4-O-methyl-α-D-glucopyranoside

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Chemical Property of methyl 2,3-di-O-benzyl-6-chloroacetamido-6-deoxy-4-O-methyl-α-D-glucopyranoside

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Technology Process of methyl 2,3-di-O-benzyl-6-chloroacetamido-6-deoxy-4-O-methyl-α-D-glucopyranoside

There total 5 articles about methyl 2,3-di-O-benzyl-6-chloroacetamido-6-deoxy-4-O-methyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 79-04-9
chloroacetyl chloride

: 193287-46-6
methyl 6-amino-2,3-di-O-benzyl-6-deoxy-4-O-methyl-α-D-glucopyranoside

: 193287-50-2
methyl 2,3-di-O-benzyl-6-chloroacetamido-6-deoxy-4-O-methyl-α-D-glucopyranoside

Guidance literature:: With triethylamine; In dichloromethane; for 2h;
DOI:10.1016/S0008-6215(97)00091-8

Reference yield:

: 67776-12-9
methyl 2,3-di-O-benzyl-6-chloro-6-deoxy-α-D-glucopyranoside

: 193287-50-2
methyl 2,3-di-O-benzyl-6-chloroacetamido-6-deoxy-4-O-methyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / NaOH / dioxane

2: 96 percent / NaN₃; tetramethylurea / dimethylformamide / 120 °C

3: 99 percent / Et₃N; H₂ / palladium on charcoal / methanol / 24 h

4: 83 percent / Et₃N / CH₂Cl₂ / 2 h

With sodium hydroxide; sodium azide; hydrogen; triethylamine; tetramethylurea; palladium on activated charcoal; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; 1: Methylation / 2: Substitution / 3: Reduction / 4: Acylation;
DOI:10.1016/S0008-6215(97)00091-8

Reference yield:

: 193287-44-4
methyl 6-azido-2,3-di-O-benzyl-6-deoxy-4-O-methyl-α-D-glucopyranoside

: 193287-50-2
methyl 2,3-di-O-benzyl-6-chloroacetamido-6-deoxy-4-O-methyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / Et₃N; H₂ / palladium on charcoal / methanol / 24 h

2: 83 percent / Et₃N / CH₂Cl₂ / 2 h

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; dichloromethane; 1: Reduction / 2: Acylation;
DOI:10.1016/S0008-6215(97)00091-8