C₂₃H₃₉NO

Base Information

• Chemical Name: C₂₃H₃₉NO
• CAS No.: 1229609-90-8
• Molecular Formula: C₂₃H₃₉NO
• Molecular Weight: 345.569
• Mol file: 1229609-90-8.mol

Synonyms:C₂₃H₃₉NO

Chemical Property of C₂₃H₃₉NO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₂₃H₃₉NO

There total 4 articles about C₂₃H₃₉NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

hexadecylmagnesium bromide (872-26-4) + anthranilic acid nitrile (1885-29-6) → C23H39NO (1229609-90-8)

Guidance literature:

hexadecylmagnesium bromide; anthranilic acid nitrile; In tetrahydrofuran; at 0 - 20 ℃;

With hydrogenchloride; water; In tetrahydrofuran;

With sodium hydroxide; In tetrahydrofuran; water; at 0 ℃;

DOI:10.1021/ol100954x

Reference yield:

C23H41NO (1352842-95-5) → C23H39NO (1229609-90-8)

Guidance literature:

With copper(II) chloride monohydrate; potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 24h;

DOI:10.1039/c1cc12885j

Reference yield:

2-nitro-benzaldehyde (552-89-6) → C23H39NO (1229609-90-8)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrogenchloride; iron / ethanol; water / 2 h / 80 °C

2: tetrahydrofuran; diethyl ether

3: copper(II) chloride monohydrate; potassium carbonate / N,N-dimethyl-formamide / 24 h / 60 °C

With hydrogenchloride; copper(II) chloride monohydrate; iron; potassium carbonate; In tetrahydrofuran; diethyl ether; ethanol; water; N,N-dimethyl-formamide;

DOI:10.1039/c1cc12885j

upstream raw materials:

hexadecylmagnesium bromide

anthranilic acid nitrile

C₂₃H₄₁NO

o-aminobenzaldehyde

Downstream raw materials:

4-hexadecyl-2-phenyl-quinazoline

2-phenylquinazoline

C₂₃H₄₁NO