1H,3H-Furo[3,4-c]furan-1-one, 6-(dimethylamino)-4-(trimethylsilyl)-

Base Information

Chemical Name:1H,3H-Furo[3,4-c]furan-1-one, 6-(dimethylamino)-4-(trimethylsilyl)-
CAS No.:289673-85-4
Molecular Formula:C₁₁H₁₇NO₃Si
Molecular Weight:239.346
Hs Code.:
Mol file:289673-85-4.mol

Synonyms:1H,3H-Furo[3,4-c]furan-1-one, 6-(dimethylamino)-4-(trimethylsilyl)-

Suppliers and Price of 1H,3H-Furo[3,4-c]furan-1-one, 6-(dimethylamino)-4-(trimethylsilyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H,3H-Furo[3,4-c]furan-1-one, 6-(dimethylamino)-4-(trimethylsilyl)-

Chemical Property:

PSA：0.00000
LogP:0.00000

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1H,3H-Furo[3,4-c]furan-1-one, 6-(dimethylamino)-4-(trimethylsilyl)-

There total 4 articles about 1H,3H-Furo[3,4-c]furan-1-one, 6-(dimethylamino)-4-(trimethylsilyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 289673-82-1
2-diazo-N,N-dimethylmalonamic acid 3-trimethylsilanylprop-2-ynyl ester

: 289673-85-4
6-dimethylamino-4-trimethylsilanyl-3H-furo[3,4-c]furan-1-one

Guidance literature:: With rhodium(II) acetate; In hexane; at 80 ℃; for 3h;
DOI:10.1021/ol006004q

Reference yield:

: 5272-36-6
3-trimethylsilyl-2-propyn-1-ol

: 289673-85-4
6-dimethylamino-4-trimethylsilanyl-3H-furo[3,4-c]furan-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / DMAP; 1,3-dicyclohexylcarbodiimide / CH₂Cl₂ / 3 h / 20 °C

2: 100 percent / 4-nitrobenzenesulfonyl azide; Et₃N / CH₂Cl₂ / 12 h / 0 °C

3: 98 percent / Rh₂(OAc)4 / hexane / 3 h / 80 °C

With dmap; p-nitrobenzenesulfonyl azide; triethylamine; dicyclohexyl-carbodiimide; dirhodium tetraacetate; In hexane; dichloromethane;
DOI:10.1021/jo020413d

Reference yield:

: 42783-81-3
3-(dimethylamino)-3-oxopropanoic acid

: 289673-85-4
6-dimethylamino-4-trimethylsilanyl-3H-furo[3,4-c]furan-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / DMAP; 1,3-dicyclohexylcarbodiimide / CH₂Cl₂ / 3 h / 20 °C

2: 100 percent / 4-nitrobenzenesulfonyl azide; Et₃N / CH₂Cl₂ / 12 h / 0 °C

3: 98 percent / Rh₂(OAc)4 / hexane / 3 h / 80 °C

With dmap; p-nitrobenzenesulfonyl azide; triethylamine; dicyclohexyl-carbodiimide; dirhodium tetraacetate; In hexane; dichloromethane;
DOI:10.1021/jo020413d