1-[3-[[(diphenylphosphinyl)acetyl]amino]propyl]-3-ethyl-1H-imidazol-3-ium bromide

Base Information

Chemical Name:1-[3-[[(diphenylphosphinyl)acetyl]amino]propyl]-3-ethyl-1H-imidazol-3-ium bromide
CAS No.:1228996-14-2
Molecular Formula:Br*C₂₂H₂₇N₃O₂P
Molecular Weight:476.353
Hs Code.:

Synonyms:1-[3-[[(diphenylphosphinyl)acetyl]amino]propyl]-3-ethyl-1H-imidazol-3-ium bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[3-[[(diphenylphosphinyl)acetyl]amino]propyl]-3-ethyl-1H-imidazol-3-ium bromide

Chemical Property:

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Technology Process of 1-[3-[[(diphenylphosphinyl)acetyl]amino]propyl]-3-ethyl-1H-imidazol-3-ium bromide

There total 3 articles about 1-[3-[[(diphenylphosphinyl)acetyl]amino]propyl]-3-ethyl-1H-imidazol-3-ium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 74-96-4
ethyl bromide

: 1228996-38-0
2-(diphenylphosphinyl)-N-[3-(1H-imidazol-1-yl)propyl]-acetamide

: 1228996-14-2
1-[3-[[(diphenylphosphinyl)acetyl]amino]propyl]-3-ethyl-1H-imidazol-3-ium bromide

Guidance literature:: In acetonitrile; at 0 - 85 ℃; Inert atmosphere;
DOI:10.1039/b926377b

Reference yield:

: 6361-05-3
ethyl 2-(diphenylphosphoryl)acetate

: 1228996-14-2
1-[3-[[(diphenylphosphinyl)acetyl]amino]propyl]-3-ethyl-1H-imidazol-3-ium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol; water / 72 h / Reflux; Sealed tube

2: acetonitrile / 0 - 85 °C / Inert atmosphere

In ethanol; water; acetonitrile;
DOI:10.1039/b926377b

Reference yield:

: 5036-48-6
3-(1H-imidazol-1-yl)propan-1-amine

: 1228996-14-2
1-[3-[[(diphenylphosphinyl)acetyl]amino]propyl]-3-ethyl-1H-imidazol-3-ium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol; water / 72 h / Reflux; Sealed tube

2: acetonitrile / 0 - 85 °C / Inert atmosphere

In ethanol; water; acetonitrile;
DOI:10.1039/b926377b