(2R,3R,4R)-3-(benzyloxy)-5-(tert-butyl-diphenylsilyloxy)-2,4-di-hydroxylpentyl benzoate

Base Information

Chemical Name:(2R,3R,4R)-3-(benzyloxy)-5-(tert-butyl-diphenylsilyloxy)-2,4-di-hydroxylpentyl benzoate
CAS No.:1456695-44-5
Molecular Formula:C₃₅H₄₀O₆Si
Molecular Weight:584.784
Hs Code.:

Synonyms:(2R,3R,4R)-3-(benzyloxy)-5-(tert-butyl-diphenylsilyloxy)-2,4-di-hydroxylpentyl benzoate

Suppliers and Price of (2R,3R,4R)-3-(benzyloxy)-5-(tert-butyl-diphenylsilyloxy)-2,4-di-hydroxylpentyl benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (2R,3R,4R)-3-(benzyloxy)-5-(tert-butyl-diphenylsilyloxy)-2,4-di-hydroxylpentyl benzoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of (2R,3R,4R)-3-(benzyloxy)-5-(tert-butyl-diphenylsilyloxy)-2,4-di-hydroxylpentyl benzoate

There total 3 articles about (2R,3R,4R)-3-(benzyloxy)-5-(tert-butyl-diphenylsilyloxy)-2,4-di-hydroxylpentyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1456695-43-4
(2R,3S,4R)-3-(benzyloxy)-2,4,5-trihydroxypentyl benzoate

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1456695-44-5
(2R,3R,4R)-3-(benzyloxy)-5-(tert-butyl-diphenylsilyloxy)-2,4-di-hydroxylpentyl benzoate

Guidance literature:: With 1H-imidazole; dmap; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/j.tetlet.2013.07.164

Reference yield:

: 98-88-4
benzoyl chloride

: 1456695-44-5
(2R,3R,4R)-3-(benzyloxy)-5-(tert-butyl-diphenylsilyloxy)-2,4-di-hydroxylpentyl benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; dmap / dichloromethane / 0.5 h / 0 °C

2: toluene-4-sulfonic acid / methanol / 0.5 h / 20 °C

3: dmap; 1H-imidazole / dichloromethane / 1 h / 0 °C

With pyridine; 1H-imidazole; dmap; toluene-4-sulfonic acid; In methanol; dichloromethane;
DOI:10.1016/j.tetlet.2013.07.164

Reference yield:

: 1456695-40-1
(3R)-3-(benzyloxy)-3-[(R)-2,2-diethyl-1,3-dioxolan-4-yl]propane-1,2-diol

: 1456695-44-5
(2R,3R,4R)-3-(benzyloxy)-5-(tert-butyl-diphenylsilyloxy)-2,4-di-hydroxylpentyl benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; dmap / dichloromethane / 0.5 h / 0 °C

2: toluene-4-sulfonic acid / methanol / 0.5 h / 20 °C

3: dmap; 1H-imidazole / dichloromethane / 1 h / 0 °C

With pyridine; 1H-imidazole; dmap; toluene-4-sulfonic acid; In methanol; dichloromethane;
DOI:10.1016/j.tetlet.2013.07.164