2-amino-4-(2,6-dichlorophenyl)-4H-benzo[h]chromene-3-carbonitrile

Base Information

Chemical Name:2-amino-4-(2,6-dichlorophenyl)-4H-benzo[h]chromene-3-carbonitrile
CAS No.:346436-66-6
Molecular Formula:C₂₀H₁₂Cl₂N₂O
Molecular Weight:367.234
Hs Code.:
Mol file:346436-66-6.mol

Synonyms:2-amino-4-(2,6-dichlorophenyl)-4H-benzo[h]chromene-3-carbonitrile

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Chemical Property of 2-amino-4-(2,6-dichlorophenyl)-4H-benzo[h]chromene-3-carbonitrile

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Technology Process of 2-amino-4-(2,6-dichlorophenyl)-4H-benzo[h]chromene-3-carbonitrile

There total 1 articles about 2-amino-4-(2,6-dichlorophenyl)-4H-benzo[h]chromene-3-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 90-15-3
α-naphthol

: 2972-79-4
2-(2,6-dichlorobenzylidene)malononitrile

: 346436-66-6
2-amino-4-(2,6-dichlorophenyl)-4H-benzo[h]chromene-3-carbonitrile

Guidance literature:: With piperidine; In ethanol; for 24h; Reflux;
DOI:10.1016/j.ejmech.2012.06.038

Reference yield: 70.0%

: 346436-66-6
2-amino-4-(2,6-dichlorophenyl)-4H-benzo[h]chromene-3-carbonitrile

: 108-24-7
acetic anhydride

: 7-(2,6-dichlorophenyl)-10-methyl-7H-benzo[7,8]chromeno[2,3-d]pyrimidin-8(9H)-one

Guidance literature:: With sulfuric acid; water; at 90 ℃; for 0.216667h;
DOI:10.1002/jhet.2630

Reference yield: 41.0%

: 346436-66-6
2-amino-4-(2,6-dichlorophenyl)-4H-benzo[h]chromene-3-carbonitrile

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 1393816-58-4
7-(2,6-dichlorophenyl)-9,10,11,12-tetrahydro-7H-benzo[7,8]chromeno[2,3-b]quinolin-8-amine

Guidance literature:: 2-amino-4-(2,6-dichlorophenyl)-4H-benzo[h]chromene-3-carbonitrile; cyclohexanone; With aluminum (III) chloride; In 1,4-dioxane; at 100 ℃; for 3h;

With sodium hydroxide; In 1,4-dioxane; chloroform; water; pH=11 - 12;
DOI:10.1016/j.ejmech.2012.06.038