Technology Process of C20H30O4
There total 1 articles about C20H30O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
methyl 10-chloro-10-oxodecanoate; 2,3,5-trimethylphenol;
With
aluminum (III) chloride;
In
1,1,2,2-tetrachloroethane;
at 0 - 140 ℃;
for 24h;
Inert atmosphere;
With
hydrogenchloride; water;
In
1,1,2,2-tetrachloroethane;
at 0 ℃;
Inert atmosphere;
- Guidance literature:
-
With
hydrogenchloride; mercury dichloride; zinc;
In
water; toluene;
at 20 - 140 ℃;
for 192h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogenchloride; mercury dichloride; zinc / water; toluene / 192 h / 20 - 140 °C
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere
2.2: 0 °C / Inert atmosphere
3.1: potassium nitrososulfonate; potassium hydroxide / methanol; N,N-dimethyl-formamide / 14 h / 20 °C
With
hydrogenchloride; lithium aluminium tetrahydride; potassium nitrososulfonate; mercury dichloride; potassium hydroxide; zinc;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; toluene;