Benzonitrile;iodozinc(1+)

Base Information

Chemical Name:Benzonitrile;iodozinc(1+)
CAS No.:288309-53-5
Molecular Formula:C7H4 I N Zn
Molecular Weight:294.41
Hs Code.:
DSSTox Substance ID:DTXSID10391153
Mol file:288309-53-5.mol

Synonyms:benzonitrile;iodozinc(1+);DTXSID10391153

Suppliers and Price of Benzonitrile;iodozinc(1+)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
3-Cyanophenylzinc iodide solution 0.5M in THF
50ml
$ 301.00

Rieke Metals
3-Cyanophenylzinciodide
100mL
$ 680.00

Rieke Metals
3-Cyanophenylzinciodide
50mL
$ 377.00

American Custom Chemicals Corporation
3-CYANOPHENYLZINC IODIDE 95.00%
1L
$ 10880.00

American Custom Chemicals Corporation
3-CYANOPHENYLZINC IODIDE 95.00%
500ML
$ 5640.00

American Custom Chemicals Corporation
3-CYANOPHENYLZINC IODIDE 95.00%
100ML
$ 1448.00

American Custom Chemicals Corporation
3-CYANOPHENYLZINC IODIDE 95.00%
25ML
$ 690.00

Total 8 raw suppliers

Chemical Property of Benzonitrile;iodozinc(1+)

Chemical Property:

Vapor Pressure:0.524mmHg at 25°C
Boiling Point:191.1°C at 760 mmHg
Flash Point:-17 °C
PSA：23.79000
Density:0.998 g/mL at 25 °C
LogP:2.24168
Storage Temp.:2-8°C
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:292.86799
Heavy Atom Count:10
Complexity:212

Purity/Quality:

99% ^*data from raw suppliers

3-Cyanophenylzinc iodide solution 0.5M in THF ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:F,Xn
Statements: 11-14-19-22-36/37/38-40-36/37
Safety Statements: 16-26-33-36-36/37

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C[C-]=CC(=C1)C#N.[Zn+]I
Uses 3-Cyanophenylzinc iodide can be used:As a reagent/substrate in the palladium-catalyzed synthesis of 5-substituted 2-furaldehydes of biological importance.As a substrate in the di-functionalization of indenes via α-carbonylalkylarylation to yield α-carbonyl- alkylarylated indenes.

Technology Process of Benzonitrile;iodozinc(1+)

There total 1 articles about Benzonitrile;iodozinc(1+) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69113-59-3
3-iodobenzonitrile

: 7440-66-6
zinc

: 288309-53-5
(3-cyanophenyl)zinc(II) iodide

Guidance literature:: zinc; With lithium chloride; at 150 - 170 ℃; for 2h; Schlenk technique; Inert atmosphere;

With chloro-trimethyl-silane; ethylene dibromide; In tetrahydrofuran; at 20 ℃; for 0.0833333h; Glovebox; Schlenk technique; Inert atmosphere;

3-iodobenzonitrile; In tetrahydrofuran; Glovebox; Schlenk technique; Inert atmosphere;
DOI:10.1002/anie.201913435