2-(Cyclohept-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-(Cyclohept-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:287944-13-2
Molecular Formula:C₁₃H₂₃BO₂
Molecular Weight:222.135
Hs Code.:2934999090
European Community (EC) Number:801-055-0
DSSTox Substance ID:DTXSID90573233
Nikkaji Number:J1.414.671G
Mol file:287944-13-2.mol

Synonyms:287944-13-2;2-(Cyclohept-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane;1-CYCLOHEPTENYLBORONIC ACID PINACOL ESTER;2-(cyclohepten-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane;1-CYCLOHEPTEN-1YL BORONIC ACID PINACOL ESTER;1-Cycloheptene-1-boronic Acid Pinacol Ester;MFCD10700152;1,3,2-Dioxaborolane, 2-(1-cyclohepten-1-yl)-4,4,5,5-tetramethyl-;SCHEMBL4421394;DTXSID90573233;XCKJXFSLFZYWSB-UHFFFAOYSA-N;AC8381;AKOS015999766;AB62606;BS-22211;SY066354;CS-0113003;J-017263;1-cyclohepten-1yl boronic acid pinacol ester, AldrichCPR

Suppliers and Price of 2-(Cyclohept-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
2-(Cyclohept-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane 95+%
500g
$ 109.00

Matrix Scientific
2-(Cyclohept-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane 95+%
250mg
$ 71.00

Crysdot
2-(Cyclohept-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane 95+%
5g
$ 527.00

American Custom Chemicals Corporation
1-CYCLOHEPTENYLBORONIC ACID PINACOL ESTER 95.00%
1G
$ 312.90

Alichem
2-(Cyclohept-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
5g
$ 579.88

AK Scientific
1-Cycloheptenylboronicacidpinacolester
5g
$ 1331.00

Total 17 raw suppliers

Chemical Property of 2-(Cyclohept-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Chemical Property:

Boiling Point:253.0±33.0 °C(Predicted)
PSA：18.46000
Density:0.94±0.1 g/cm3(Predicted)
LogP:3.50830
Storage Temp.:2-8°C
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:222.1791101
Heavy Atom Count:16
Complexity:278

Purity/Quality:

97% ^*data from raw suppliers

2-(Cyclohept-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B1(OC(C(O1)(C)C)(C)C)C2=CCCCCC2

Technology Process of 2-(Cyclohept-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 11 articles about 2-(Cyclohept-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 628-92-2,45509-99-7
Cycloheptene

: 73183-34-3
bis(pinacol)diborane

: 287944-13-2
2-(cyclohept-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With (CH₃Si(C₆H₄P(C₆H₃(CF₃)2)2)2)Pd(SO₃CF₃); triethylaluminum; In toluene; at 60 ℃; for 6h; Inert atmosphere;
DOI:10.1246/bcsj.20130004

Reference yield: 78.0%

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 56382-69-5
cycloheptanone p-tolylsulfonylhydrazone

: 287944-13-2
2-(cyclohept-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: cycloheptanone p-tolylsulfonylhydrazone; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In hexane; at -78 - 20 ℃; Inert atmosphere;

With Triisopropyl borate; Inert atmosphere;

2,3-dimethyl-2,3-butane diol; With hydrogenchloride; Inert atmosphere;
DOI:10.1021/ja906429c

Reference yield: 65.0%

: cyclohept-1-en-1-yl dimethylcarbamate

: 73183-34-3
bis(pinacol)diborane

: 287944-13-2
2-(cyclohept-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With iron(II) triflate; lithium methanolate; 2'-(di-tert-butylphosphanyl)-N,N-dimethyl-[1,1'-biphenyl]-2-amine; at 100 ℃; for 15h; Inert atmosphere; Schlenk technique; Glovebox;
DOI:10.1021/acs.orglett.0c01937