1-O-acetyl-2,6-anhydro-5-deoxy-3,4-O-(1-methylethylidene)-D-arabino-hex-5-enitol

Base Information

Chemical Name:1-O-acetyl-2,6-anhydro-5-deoxy-3,4-O-(1-methylethylidene)-D-arabino-hex-5-enitol
CAS No.:98815-78-2
Molecular Formula:C₁₁H₁₆O₅
Molecular Weight:228.245
Hs Code.:

Synonyms:1-O-acetyl-2,6-anhydro-5-deoxy-3,4-O-(1-methylethylidene)-D-arabino-hex-5-enitol

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Chemical Property of 1-O-acetyl-2,6-anhydro-5-deoxy-3,4-O-(1-methylethylidene)-D-arabino-hex-5-enitol

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Technology Process of 1-O-acetyl-2,6-anhydro-5-deoxy-3,4-O-(1-methylethylidene)-D-arabino-hex-5-enitol

There total 1 articles about 1-O-acetyl-2,6-anhydro-5-deoxy-3,4-O-(1-methylethylidene)-D-arabino-hex-5-enitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 124477-05-0
2,6-di-O-acetyl-3,4-O-isopropylidene-β-D-galactopyranosyl phenyl sulphone

: 98815-78-2
1-O-acetyl-2,6-anhydro-5-deoxy-3,4-O-(1-methylethylidene)-D-arabino-hex-5-enitol

: 124477-12-9
2,6-anhydro-5-deoxy-3,4-O-isopropylidene-D-arabino-hex-5-enitol

Guidance literature:: With naphthalen-1-yl-lithium; In tetrahydrofuran; at -78 - 25 ℃; for 0.25h;
DOI:10.1016/0008-6215(89)84061-3

Reference yield: 91.0%

: 71098-88-9
N-phenylselanylphthalimide

: 98815-78-2
1-O-acetyl-2,6-anhydro-5-deoxy-3,4-O-(1-methylethylidene)-D-arabino-hex-5-enitol

: 161822-66-8
Phenyl 6-O-acetyl-2-azido-2-deoxy-3,4-O-isopropylidene-1-seleno-α-D-galactopyranoside

Guidance literature:: With trimethylsilylazide; tetrabutyl ammonium fluoride; In dichloromethane; for 48h; Ambient temperature;
DOI:10.1139/v95-046

Reference yield: 84.0%

: 21368-28-5
4-chlorobenzoyl azide

: 98815-78-2
1-O-acetyl-2,6-anhydro-5-deoxy-3,4-O-(1-methylethylidene)-D-arabino-hex-5-enitol

: C₁₈H₂₀ClNO₆

Guidance literature:: With dichloro(meso-tetrakis(4-tolyl)porphyrinato)ruthenium(IV); In 1,2-dichloro-ethane; at 70 ℃; for 12h; Molecular sieve; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.202100668