DIPHENYL-D10-AMINE

Base Information

• Chemical Name: DIPHENYL-D10-AMINE
• CAS No.: 37055-51-9
• Molecular Formula: C12H D10 N
• Molecular Weight: 179.147
• Mol file: 37055-51-9.mol

Synonyms:Benzen-d5-amine,N-(phenyl-d5)- (9CI)

Chemical Property of DIPHENYL-D10-AMINE

Chemical Property:

• PSA: 12.03000
• LogP: 3.50320

Purity/Quality:

99%, ^*data from raw suppliers

Diphenylamine-d10 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: Diphenylamine-d10 is the isotope labelled analogue of Diphenylamine (D478940), an aromatic amine that was shown to exhibit antioxidant activities and is now used as an anti-scald agent.

Technology Process of DIPHENYL-D10-AMINE

There total 5 articles about DIPHENYL-D10-AMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

bromobenzene-d5 (4165-57-5) + aniline-d5 (4165-61-1) → d10-diphenylamine (37055-51-9)

Guidance literature:

With tri-tert-butyl phosphine; sodium t-butanolate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In toluene; for 3h; Heating / reflux;

Reference yield: 72.0%

diphenylamine (122-39-4) → d10-diphenylamine (37055-51-9)

Guidance literature:

With 10% Pt/activated carbon; palladium 10% on activated carbon; hydrogen; water-d2; at 80 ℃; for 4h;

DOI:10.3390/molecules191118604

Reference yield: 64.0%

diphenylamine (122-39-4) → carbazole-d8 (38537-24-5) + d10-diphenylamine (37055-51-9)

Guidance literature:

With water-d2; platinum on activated charcoal; at 250 ℃; for 2h;

DOI:10.1246/cl.2007.172

upstream raw materials:

diphenylamine

bromobenzene-d5

aniline-d5

nitrobenzene-d5

Downstream raw materials:

C₇₂H₃⁽²⁾H₄₅N₂

C₈₄H₃⁽²⁾H₅₄N₃

1,4-diphenyl-1H-quinolin-2-one