(2-chloro-9H-fluoren-9-yl)methyl 4-methoxybenzylcarbamate

Base Information

Chemical Name:(2-chloro-9H-fluoren-9-yl)methyl 4-methoxybenzylcarbamate
CAS No.:1329489-81-7
Molecular Formula:C₂₃H₂₀ClNO₃
Molecular Weight:393.87
Hs Code.:

Synonyms:(2-chloro-9H-fluoren-9-yl)methyl 4-methoxybenzylcarbamate

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Chemical Property of (2-chloro-9H-fluoren-9-yl)methyl 4-methoxybenzylcarbamate

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Technology Process of (2-chloro-9H-fluoren-9-yl)methyl 4-methoxybenzylcarbamate

There total 5 articles about (2-chloro-9H-fluoren-9-yl)methyl 4-methoxybenzylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1329489-24-8
methyl 2-(4'-chlorobiphenyl-2-yl)diazoacetate

: 1329489-81-7
(2-chloro-9H-fluoren-9-yl)methyl 4-methoxybenzylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: dirhodium tetraacetate / 1,2-dichloro-ethane / 1 h / 25 °C / Inert atmosphere

2: diisobutylaluminium hydride

With dirhodium tetraacetate; diisobutylaluminium hydride; In 1,2-dichloro-ethane;
DOI:10.1002/asia.201100142

Reference yield:

: 1329489-84-0
methyl 2-(4'-chlorobiphenyl-2-yl)acetate

: 1329489-81-7
(2-chloro-9H-fluoren-9-yl)methyl 4-methoxybenzylcarbamate

Guidance literature:: Multi-step reaction with 5 steps

1.1: 4-acetamidobenzenesulfonyl azide / tetrahydrofuran / 0.08 h / Inert atmosphere

1.2: 12 h / 25 °C / Inert atmosphere

2.1: dirhodium tetraacetate / 1,2-dichloro-ethane / 1 h / 25 °C / Inert atmosphere

3.1: diisobutylaluminium hydride

With dirhodium tetraacetate; 4-acetamidobenzenesulfonyl azide; diisobutylaluminium hydride; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1002/asia.201100142

Reference yield:

: 57486-69-8
methyl 2-(2-bromophenyl)acetate

: 1329489-81-7
(2-chloro-9H-fluoren-9-yl)methyl 4-methoxybenzylcarbamate

Guidance literature:: Multi-step reaction with 6 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 0.08 h

1.2: 12 h / 100 °C

2.1: 4-acetamidobenzenesulfonyl azide / tetrahydrofuran / 0.08 h / Inert atmosphere

2.2: 12 h / 25 °C / Inert atmosphere

3.1: dirhodium tetraacetate / 1,2-dichloro-ethane / 1 h / 25 °C / Inert atmosphere

4.1: diisobutylaluminium hydride

With dirhodium tetraacetate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 4-acetamidobenzenesulfonyl azide; diisobutylaluminium hydride; potassium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; water; 1,2-dichloro-ethane; 1.2: Suzuki-Miyaura coupling;
DOI:10.1002/asia.201100142