d₂₂-2,4,6-trimethyl-N-[2-[(2,4,6-trimethylphenyl) imino]ethylidene]aniline

Base Information

Chemical Name:d₂₂-2,4,6-trimethyl-N-[2-[(2,4,6-trimethylphenyl) imino]ethylidene]aniline
CAS No.:1126138-21-3
Molecular Formula:C₂₀H₂₄N₂
Molecular Weight:314.249
Hs Code.:

d<sub>22</sub>-2,4,6-trimethyl-N-[2-[(2,4,6-trimethylphenyl) imino]ethylidene]aniline

Synonyms:d₂₂-2,4,6-trimethyl-N-[2-[(2,4,6-trimethylphenyl) imino]ethylidene]aniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of d₂₂-2,4,6-trimethyl-N-[2-[(2,4,6-trimethylphenyl) imino]ethylidene]aniline

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Technology Process of d₂₂-2,4,6-trimethyl-N-[2-[(2,4,6-trimethylphenyl) imino]ethylidene]aniline

There total 3 articles about d₂₂-2,4,6-trimethyl-N-[2-[(2,4,6-trimethylphenyl) imino]ethylidene]aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 131543-46-9,107-22-2
Glyoxal

: 1126138-13-3
d₁₁-2,4,6-trimethylaniline

: 1126138-21-3
d₂₂-2,4,6-trimethyl-N-[2-[(2,4,6-trimethylphenyl) imino]ethylidene]aniline

Guidance literature:: In water; isopropyl alcohol;
DOI:10.1002/chem.200801584

Reference yield:

: 1126138-12-2
d₁₁-1,3,5-trimethyl-2-nitrobenzene

: 1126138-21-3
d₂₂-2,4,6-trimethyl-N-[2-[(2,4,6-trimethylphenyl) imino]ethylidene]aniline

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; zinc / ethanol / 5 h / 20 °C

2: formic acid / methanol / 16 h / 20 °C

With formic acid; acetic acid; zinc; In methanol; ethanol;
DOI:10.1021/ic401783c

Reference yield:

: 69441-16-3
perdeuterio-1,3,5-trimethylbenzene

: 1126138-21-3
d₂₂-2,4,6-trimethyl-N-[2-[(2,4,6-trimethylphenyl) imino]ethylidene]aniline

Guidance literature:: Multi-step reaction with 3 steps

1: nitric acid / acetic anhydride / 1 h / 20 °C

2: acetic acid; zinc / ethanol / 5 h / 20 °C

3: formic acid / methanol / 16 h / 20 °C

With formic acid; nitric acid; acetic acid; zinc; In methanol; ethanol; acetic anhydride;
DOI:10.1021/ic401783c