ELX-05

Base Information

Chemical Name:ELX-05
CAS No.:1356826-89-5
Molecular Formula:C₁₈H₃₆N₄O₁₀
Molecular Weight:468.505
Hs Code.:

Synonyms:ELX-05

Suppliers and Price of ELX-05

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ELX-05

Chemical Property:

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Technology Process of ELX-05

There total 14 articles about ELX-05 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 5-O-(5-azido-5,6-dideoxy-2,3-O-dibenzoyl-α-L-talofuranosyl)-3',4',6',6-tetra-O-acetyl-2',1,3-triazido paromamine

: 1356826-89-5
ELX-05

Guidance literature:: 5-O-(5-azido-5,6-dideoxy-2,3-O-dibenzoyl-α-L-talofuranosyl)-3',4',6',6-tetra-O-acetyl-2',1,3-triazido paromamine; With ethanol; methylamine; for 8h;

With water; sodium hydroxide; In tetrahydrofuran; at 20 ℃; for 0.166667h;

With trimethylphosphane; In tetrahydrofuran;

Reference yield:

: 1356826-95-3
4-methylphenyl 6-deoxy-2,3-O-1-methylethylidene-1-thio-β-Dallofuranoside

: 1356826-89-5
ELX-05

Guidance literature:: Multi-step reaction with 7 steps

1.1: pyridine / dmap / 0 - 20 °C

2.1: N,N,N,N,N,N-hexamethylphosphoric triamide; sodium azide / N,N-dimethyl-formamide / 20 - 70 °C

3.1: water; acetic acid / 70 °C

4.1: pyridine / dmap / 0 - 20 °C

5.1: N-Bromosuccinimide / water; acetone / -30 °C

5.2: 0 °C

6.1: dichloromethane / 0.17 h / -20 °C / 4 ? Molecular sieve

6.2: 1 h / -15 °C

7.1: ethanol; methylamine / 8 h

7.2: 0.17 h / 20 °C

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; N-Bromosuccinimide; sodium azide; ethanol; water; acetic acid; methylamine; dmap; In dichloromethane; water; N,N-dimethyl-formamide; acetone;

Reference yield:

: 1356826-97-5
4-methylphenyl 6-deoxy-5-O-tosyl-2,3-O-1-methylethylidene-1-thio-β-D-allofuranoside

: 1356826-89-5
ELX-05

Guidance literature:: Multi-step reaction with 6 steps

1.1: N,N,N,N,N,N-hexamethylphosphoric triamide; sodium azide / N,N-dimethyl-formamide / 20 - 70 °C

2.1: water; acetic acid / 70 °C

3.1: pyridine / dmap / 0 - 20 °C

4.1: N-Bromosuccinimide / water; acetone / -30 °C

4.2: 0 °C

5.1: dichloromethane / 0.17 h / -20 °C / 4 ? Molecular sieve

5.2: 1 h / -15 °C

6.1: ethanol; methylamine / 8 h

6.2: 0.17 h / 20 °C

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; N-Bromosuccinimide; sodium azide; ethanol; water; acetic acid; methylamine; dmap; In dichloromethane; water; N,N-dimethyl-formamide; acetone;