4-methylphenyl 6-deoxy-2,3-O-1-methylethylidene-1-thio-β-Dallofuranoside

Base Information

Chemical Name:4-methylphenyl 6-deoxy-2,3-O-1-methylethylidene-1-thio-β-Dallofuranoside
CAS No.:1356826-95-3
Molecular Formula:C₁₆H₂₂O₄S
Molecular Weight:310.414
Hs Code.:

Synonyms:4-methylphenyl 6-deoxy-2,3-O-1-methylethylidene-1-thio-β-Dallofuranoside

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Chemical Property of 4-methylphenyl 6-deoxy-2,3-O-1-methylethylidene-1-thio-β-Dallofuranoside

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Technology Process of 4-methylphenyl 6-deoxy-2,3-O-1-methylethylidene-1-thio-β-Dallofuranoside

There total 3 articles about 4-methylphenyl 6-deoxy-2,3-O-1-methylethylidene-1-thio-β-Dallofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1356826-94-2
4-methylphenyl 2,3-O-1-methylethylidene-1-thio-β-D-ribopentodialdo-1,4-furanoside

: 75-16-1
methylmagnesium bromide

: 1356826-96-4
4-methylphenyl 6-deoxy-2,3-O-1-methylethylidene-1-thio-α-L-allofuranoside

: 1356826-95-3
4-methylphenyl 6-deoxy-2,3-O-1-methylethylidene-1-thio-β-Dallofuranoside

Guidance literature:: 4-methylphenyl 2,3-O-1-methylethylidene-1-thio-β-D-ribopentodialdo-1,4-furanoside; methylmagnesium bromide; In tetrahydrofuran; at -30 ℃; for 2.5h;

With ammonium chloride; In tetrahydrofuran; water;

Reference yield:

: 1131610-84-8
p-tolyl 1-thio-β-D-ribofuranoside

: 1356826-95-3
4-methylphenyl 6-deoxy-2,3-O-1-methylethylidene-1-thio-β-Dallofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: magnesium sulfate / (1S)-10-camphorsulfonic acid / acetone / 5 h / 20 °C

2: magnesium sulfate; Dess-Martin periodane / dichloromethane / 8 h / 20 °C

3: tetrahydrofuran / 2.5 h / -30 °C

With magnesium sulfate; Dess-Martin periodane; (1S)-10-camphorsulfonic acid; In tetrahydrofuran; dichloromethane; acetone;

Reference yield:

: C₁₅H₂₀O₄S

: 1356826-95-3
4-methylphenyl 6-deoxy-2,3-O-1-methylethylidene-1-thio-β-Dallofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: magnesium sulfate; Dess-Martin periodane / dichloromethane / 8 h / 20 °C

2: tetrahydrofuran / 2.5 h / -30 °C

With magnesium sulfate; Dess-Martin periodane; In tetrahydrofuran; dichloromethane;