4-methylphenyl 6-deoxy-5-O-tosyl-2,3-O-1-methylethylidene-1-thio-β-D-allofuranoside

Base Information

Chemical Name:4-methylphenyl 6-deoxy-5-O-tosyl-2,3-O-1-methylethylidene-1-thio-β-D-allofuranoside
CAS No.:1356826-97-5
Molecular Formula:C₂₃H₂₈O₆S₂
Molecular Weight:464.604
Hs Code.:

Synonyms:4-methylphenyl 6-deoxy-5-O-tosyl-2,3-O-1-methylethylidene-1-thio-β-D-allofuranoside

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Chemical Property of 4-methylphenyl 6-deoxy-5-O-tosyl-2,3-O-1-methylethylidene-1-thio-β-D-allofuranoside

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Technology Process of 4-methylphenyl 6-deoxy-5-O-tosyl-2,3-O-1-methylethylidene-1-thio-β-D-allofuranoside

There total 4 articles about 4-methylphenyl 6-deoxy-5-O-tosyl-2,3-O-1-methylethylidene-1-thio-β-D-allofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1356826-95-3
4-methylphenyl 6-deoxy-2,3-O-1-methylethylidene-1-thio-β-Dallofuranoside

: 98-59-9
p-toluenesulfonyl chloride

: 1356826-97-5
4-methylphenyl 6-deoxy-5-O-tosyl-2,3-O-1-methylethylidene-1-thio-β-D-allofuranoside

Guidance literature:: With pyridine; dmap; at 0 - 20 ℃;

Reference yield:

: 1131610-84-8
p-tolyl 1-thio-β-D-ribofuranoside

: 1356826-97-5
4-methylphenyl 6-deoxy-5-O-tosyl-2,3-O-1-methylethylidene-1-thio-β-D-allofuranoside

Guidance literature:: Multi-step reaction with 4 steps

1: magnesium sulfate / (1S)-10-camphorsulfonic acid / acetone / 5 h / 20 °C

2: magnesium sulfate; Dess-Martin periodane / dichloromethane / 8 h / 20 °C

3: tetrahydrofuran / 2.5 h / -30 °C

4: pyridine / dmap / 0 - 20 °C

With pyridine; magnesium sulfate; Dess-Martin periodane; dmap; (1S)-10-camphorsulfonic acid; In tetrahydrofuran; dichloromethane; acetone;

Reference yield:

: 1356826-94-2
4-methylphenyl 2,3-O-1-methylethylidene-1-thio-β-D-ribopentodialdo-1,4-furanoside

: 1356826-97-5
4-methylphenyl 6-deoxy-5-O-tosyl-2,3-O-1-methylethylidene-1-thio-β-D-allofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 2.5 h / -30 °C

2: pyridine / dmap / 0 - 20 °C

With pyridine; dmap; In tetrahydrofuran;