Carbamic acid, [(1S)-1-(2-hydroxyethyl)-2-propenyl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, [(1S)-1-(2-hydroxyethyl)-2-propenyl]-, 1,1-dimethylethyl ester
CAS No.:286949-39-1
Molecular Formula:C10H19 N O3
Molecular Weight:201.266
Hs Code.:
Mol file:286949-39-1.mol

Synonyms:Carbamic acid, [(1S)-1-(2-hydroxyethyl)-2-propenyl]-, 1,1-dimethylethyl ester

Suppliers and Price of Carbamic acid, [(1S)-1-(2-hydroxyethyl)-2-propenyl]-, 1,1-dimethylethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of Carbamic acid, [(1S)-1-(2-hydroxyethyl)-2-propenyl]-, 1,1-dimethylethyl ester

Chemical Property:

PSA：58.56000
LogP:1.83900

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, [(1S)-1-(2-hydroxyethyl)-2-propenyl]-, 1,1-dimethylethyl ester

There total 2 articles about Carbamic acid, [(1S)-1-(2-hydroxyethyl)-2-propenyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 24424-99-5
di-tert-butyl dicarbonate

: (S)-3-aminopent-4-en-1-ol

: 286949-39-1
1-(1,1-dimethylethoxy)-N-(1-(2-hydroxyethyl)-2-propenyl)methanamide

Guidance literature:: With triethylamine; In ethanol; at 20 ℃; for 18h;
DOI:10.1021/acs.joc.7b01181

Reference yield: 82.0%

: (2-hydroxy-tetrahydro-furan-3-yl)-carbamic acid tert-butyl ester

: 1779-49-3
Methyltriphenylphosphonium bromide

: 286949-39-1
1-(1,1-dimethylethoxy)-N-(1-(2-hydroxyethyl)-2-propenyl)methanamide

Guidance literature:: Methyltriphenylphosphonium bromide; With sodium amide; In dichloromethane;

(2-hydroxy-tetrahydro-furan-3-yl)-carbamic acid tert-butyl ester; In dichloromethane; toluene; for 4h; Heating;

In dichloromethane; toluene; at 20 ℃; for 72h; Further stages.;
DOI:10.1021/ol005903b

Reference yield: 92.0%

: 286949-39-1
1-(1,1-dimethylethoxy)-N-(1-(2-hydroxyethyl)-2-propenyl)methanamide

: 100-39-0
benzyl bromide

: 286949-40-4
[1-(2-benzyloxy-ethyl)-allyl]-carbamic acid tert-butyl ester

Guidance literature:: 1-(1,1-dimethylethoxy)-N-(1-(2-hydroxyethyl)-2-propenyl)methanamide; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.25h;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; Further stages.;
DOI:10.1021/ol005903b