Fe2(μ-H)(propanedithiolate)(CO)2(cis-1,2-bis(diphenylphosphino)ethene)]BF4

Base Information

• Chemical Name: Fe2(μ-H)(propanedithiolate)(CO)2(cis-1,2-bis(diphenylphosphino)ethene)]BF4
• CAS No.: 1019850-43-1
• Molecular Formula: BF₄*C₅₇H₅₁Fe₂O₂P₄S₂
• Molecular Weight: 1154.56

Synonyms:Fe2(μ-H)(propanedithiolate)(CO)2(cis-1,2-bis(diphenylphosphino)ethene)]BF4

Chemical Property of Fe2(μ-H)(propanedithiolate)(CO)2(cis-1,2-bis(diphenylphosphino)ethene)]BF4

Chemical Property:

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Technology Process of Fe2(μ-H)(propanedithiolate)(CO)2(cis-1,2-bis(diphenylphosphino)ethene)]BF4

There total 2 articles about Fe2(μ-H)(propanedithiolate)(CO)2(cis-1,2-bis(diphenylphosphino)ethene)]BF4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

carbon monoxide (201230-82-2) + C56H52Fe2OP4S2 → Fe2(μ-H)(propanedithiolate)(CO)2(cis-1,2-bis(diphenylphosphino)ethene)]BF4 (1019850-43-1)

Guidance literature:

In tetrahydrofuran; at 20 ℃; under 310.297 Torr; Inert atmosphere;

DOI:10.1021/ja501366j

Reference yield:

tetrafluoroboric acid diethyl ether (67969-82-8) + Fe2(pdt)(CO)2(cis-1,2-bis(diphenylphosphino)ethylene)2 (945735-90-0) → Fe2(μ-H)(propanedithiolate)(CO)2(cis-1,2-bis(diphenylphosphino)ethene)]BF4 (1019850-43-1)

Guidance literature:

In not given; treatment of iron compd. with tetrafluoroboronic acid at low temp., warming to 20°C; not isolated, NMR; Kinetics;

DOI:10.1021/ic800030y

Reference yield: 88.0%

Fe2(μ-H)(propanedithiolate)(CO)2(cis-1,2-bis(diphenylphosphino)ethene)]BF4 (1019850-43-1) + acetonitrile (75-05-8,26809-02-9) → C58H54Fe2NOP4S2(1+)*BF4(1-)

Guidance literature:

In dichloromethane; for 6h; Irradiation; Schlenk technique; Inert atmosphere;

DOI:10.1021/ja501366j

upstream raw materials:

tetrafluoroboric acid diethyl ether

Fe₂(pdt)(CO)₂(cis-1,2-bis(diphenylphosphino)ethylene)2

carbon monoxide

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