Technology Process of C29H40N2O2
There total 7 articles about C29H40N2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
boron trifluoride diethyl etherate;
In
diethyl ether; toluene;
at 118 ℃;
stereoselective reaction;
Inert atmosphere;
DOI:10.1016/j.ejmech.2013.04.044
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine / 18 h / 20 °C
2: sodium hydroxide / acetonitrile / 3 h / 20 °C
3: sodium acetate / ethanol / 78 °C
4: boron trifluoride diethyl etherate / toluene; diethyl ether / 118 °C / Inert atmosphere
With
pyridine; boron trifluoride diethyl etherate; sodium acetate; sodium hydroxide;
In
diethyl ether; ethanol; toluene; acetonitrile;
DOI:10.1016/j.ejmech.2013.04.044
- Guidance literature:
-
Multi-step reaction with 7 steps
1: sulfuric acid
2: potassium hydroxide / dimethyl sulfoxide / 3 h / 20 °C
3: sodium ethanolate / ethanol; water / 3 h / 60 °C
4: pyridine / 18 h / 20 °C
5: sodium hydroxide / acetonitrile / 3 h / 20 °C
6: sodium acetate / ethanol / 78 °C
7: boron trifluoride diethyl etherate / toluene; diethyl ether / 118 °C / Inert atmosphere
With
pyridine; sulfuric acid; boron trifluoride diethyl etherate; sodium ethanolate; sodium acetate; potassium hydroxide; sodium hydroxide;
In
diethyl ether; ethanol; water; dimethyl sulfoxide; toluene; acetonitrile;
DOI:10.1016/j.ejmech.2013.04.044
