acetic acid 2,4,6-triiodophenyl ester

Base Information

• Chemical Name: acetic acid 2,4,6-triiodophenyl ester
• CAS No.: 957137-55-2
• Molecular Formula: C₈H₅I₃O₂
• Molecular Weight: 513.84
• Mol file: 957137-55-2.mol

Synonyms:acetic acid 2,4,6-triiodophenyl ester

Chemical Property of acetic acid 2,4,6-triiodophenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of acetic acid 2,4,6-triiodophenyl ester

There total 4 articles about acetic acid 2,4,6-triiodophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2,4,6-Triiodophenol (609-23-4,72100-00-6) + acetic anhydride (108-24-7) → acetic acid 2,4,6-triiodophenyl ester (957137-55-2)

Guidance literature:

With silver trifluoromethanesulfonate; at 60 ℃; for 0.0833333h; neat (no solvent);

DOI:10.1055/s-0030-1259999

Reference yield:

2,4,6-Triiodophenol (609-23-4,72100-00-6) + acetyl chloride (75-36-5) → acetic acid 2,4,6-triiodophenyl ester (957137-55-2)

Guidance literature:

With triethylamine;

DOI:10.1021/ol050876g

Reference yield:

phenol (108-95-2,27073-41-2) → acetic acid 2,4,6-triiodophenyl ester (957137-55-2)

Guidance literature:

Multi-step reaction with 2 steps

1: alkali / durch Jodierung

2: concentrated sulfuric acid

With sulfuric acid;

upstream raw materials:

2,4,6-Triiodophenol

acetic anhydride

acetyl chloride

phenol

Downstream raw materials:

2,4,6-tri-hex-1-ynyl-phenol