ethyl 4-{(4-bromo-2-formylphenyl)[(4-methylphenyl)sulfonyl]amino}butanoate

Base Information

Chemical Name:ethyl 4-{(4-bromo-2-formylphenyl)[(4-methylphenyl)sulfonyl]amino}butanoate
CAS No.:943819-82-7
Molecular Formula:C₂₀H₂₂BrNO₅S
Molecular Weight:468.368
Hs Code.:

Synonyms:ethyl 4-{(4-bromo-2-formylphenyl)[(4-methylphenyl)sulfonyl]amino}butanoate

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Chemical Property of ethyl 4-{(4-bromo-2-formylphenyl)[(4-methylphenyl)sulfonyl]amino}butanoate

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Technology Process of ethyl 4-{(4-bromo-2-formylphenyl)[(4-methylphenyl)sulfonyl]amino}butanoate

There total 9 articles about ethyl 4-{(4-bromo-2-formylphenyl)[(4-methylphenyl)sulfonyl]amino}butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 2969-81-5
Ethyl 4-bromobutyrate

: 34159-05-2
N-(4-bromo-2-formylphenyl)-4-methylbenzenesulfonamide

: 943819-82-7
ethyl 4-{(4-bromo-2-formylphenyl)[(4-methylphenyl)sulfonyl]amino}butanoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 4h;
DOI:10.3987/COM-07-11025

Reference yield: 31.0%

: ethyl 4-(4-bromo-2-formylphenyl)aminobutyrate

: 98-59-9
p-toluenesulfonyl chloride

: 943819-82-7
ethyl 4-{(4-bromo-2-formylphenyl)[(4-methylphenyl)sulfonyl]amino}butanoate

Guidance literature:: In pyridine; at 50 ℃; for 62h;

Reference yield:

: 5344-90-1
2-Aminobenzyl alcohol

: 943819-82-7
ethyl 4-{(4-bromo-2-formylphenyl)[(4-methylphenyl)sulfonyl]amino}butanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / pyridine / tetrahydrofuran / 1.5 h / 20 °C

2: 80 percent / MnO₂ / acetone / 15 h / 20 °C

3: 93 percent / AcONa; Br₂ / acetic acid; H₂O / 4 h / 20 °C

4: 89 percent / K₂CO₃ / dimethylformamide / 4 h / 70 °C

With pyridine; manganese(IV) oxide; bromine; sodium acetate; potassium carbonate; In tetrahydrofuran; water; acetic acid; N,N-dimethyl-formamide; acetone;
DOI:10.3987/COM-07-11025