Thiophosphoric acid O-[(2R,3R,4R,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-[3-(4-methoxy-benzoyl)-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl]-4-(tetrahydro-pyran-2-yloxy)-tetrahydro-furan-3-yl] ester S-phenyl ester

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Chemical Name:Thiophosphoric acid O-[(2R,3R,4R,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-[3-(4-methoxy-benzoyl)-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl]-4-(tetrahydro-pyran-2-yloxy)-tetrahydro-furan-3-yl] ester S-phenyl ester
CAS No.:86964-79-6
Molecular Formula:C₄₉H₄₉N₂O₁₃PS
Molecular Weight:936.973
Hs Code.:

Thiophosphoric acid O-[(2R,3R,4R,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-[3-(4-methoxy-benzoyl)-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl]-4-(tetrahydro-pyran-2-yloxy)-tetrahydro-furan-3-yl] ester S-phenyl ester

Synonyms:Thiophosphoric acid O-[(2R,3R,4R,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-[3-(4-methoxy-benzoyl)-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl]-4-(tetrahydro-pyran-2-yloxy)-tetrahydro-furan-3-yl] ester S-phenyl ester

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Chemical Property of Thiophosphoric acid O-[(2R,3R,4R,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-[3-(4-methoxy-benzoyl)-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl]-4-(tetrahydro-pyran-2-yloxy)-tetrahydro-furan-3-yl] ester S-phenyl ester

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Technology Process of Thiophosphoric acid O-[(2R,3R,4R,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-[3-(4-methoxy-benzoyl)-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl]-4-(tetrahydro-pyran-2-yloxy)-tetrahydro-furan-3-yl] ester S-phenyl ester

There total 3 articles about Thiophosphoric acid O-[(2R,3R,4R,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-[3-(4-methoxy-benzoyl)-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl]-4-(tetrahydro-pyran-2-yloxy)-tetrahydro-furan-3-yl] ester S-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86964-78-5
S,S-diphenyl 2'-O-(tetrahydropyran-2-yl)-5'-O-(4,4'-dimethoxytrityl)-N³-anisoyluridine-3'-phosphorodithioate

: 86964-79-6
Thiophosphoric acid O-[(2R,3R,4R,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-[3-(4-methoxy-benzoyl)-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl]-4-(tetrahydro-pyran-2-yloxy)-tetrahydro-furan-3-yl] ester S-phenyl ester

Guidance literature:: With hypophosphorous acid; triethylamine; In pyridine; at 40 ℃; for 0.166667h;
DOI:10.1246/cl.1983.1051

Reference yield:

: 100-07-2
4-methoxy-benzoyl chloride

: 86964-79-6
Thiophosphoric acid O-[(2R,3R,4R,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-[3-(4-methoxy-benzoyl)-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl]-4-(tetrahydro-pyran-2-yloxy)-tetrahydro-furan-3-yl] ester S-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / ethyldiisopropylamine / pyridine / 15 h / Ambient temperature

2: 4 M phosphinic acid, triethylamine / pyridine / 0.17 h / 40 °C

With hypophosphorous acid; triethylamine; N-ethyl-N,N-diisopropylamine; In pyridine;
DOI:10.1246/cl.1983.1051

Reference yield:

: 81244-07-7
Dithiophosphoric acid O-[(2R,3R,4R,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-4-(tetrahydro-pyran-2-yloxy)-tetrahydro-furan-3-yl] ester S,S'-diphenyl ester

: 86964-79-6
Thiophosphoric acid O-[(2R,3R,4R,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-[3-(4-methoxy-benzoyl)-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl]-4-(tetrahydro-pyran-2-yloxy)-tetrahydro-furan-3-yl] ester S-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / ethyldiisopropylamine / pyridine / 15 h / Ambient temperature

2: 4 M phosphinic acid, triethylamine / pyridine / 0.17 h / 40 °C

With hypophosphorous acid; triethylamine; N-ethyl-N,N-diisopropylamine; In pyridine;
DOI:10.1246/cl.1983.1051