Carbamic acid, (2-isocyanatoethyl)-, 1,1-dimethylethyl ester (9CI)

Base Information

Chemical Name:Carbamic acid, (2-isocyanatoethyl)-, 1,1-dimethylethyl ester (9CI)
CAS No.:284049-22-5
Molecular Formula:C8H14 N2 O3
Molecular Weight:186.20836
Hs Code.:
Mol file:284049-22-5.mol

Synonyms:Carbamicacid, (2-isocyanatoethyl)-, 1,1-dimethylethyl ester (9CI)

Suppliers and Price of Carbamic acid, (2-isocyanatoethyl)-, 1,1-dimethylethyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1,1-DIMETHYLETHYL-(2-ISOCYANATOETHYL)CARBAMIC ACID ESTER 95.00%
5MG
$ 497.02

Total 4 raw suppliers

Chemical Property of Carbamic acid, (2-isocyanatoethyl)-, 1,1-dimethylethyl ester (9CI)

Chemical Property:

Boiling Point:276.4±23.0 °C(Predicted)
PKA:12.12±0.46(Predicted)
PSA：71.25000
Density:1.06±0.1 g/cm3(Predicted)
LogP:1.05130

Purity/Quality:

97% ^*data from raw suppliers

1,1-DIMETHYLETHYL-(2-ISOCYANATOETHYL)CARBAMIC ACID ESTER 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses tert-Butyl N-(2-Isocyanatoethyl)carbamate, Technical Grade can be used to treat cancer, fatty liver, or inflammation.

Technology Process of Carbamic acid, (2-isocyanatoethyl)-, 1,1-dimethylethyl ester (9CI)

There total 5 articles about Carbamic acid, (2-isocyanatoethyl)-, 1,1-dimethylethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 32315-10-9
bis(trichloromethyl) carbonate

: 57260-73-8
N-BOC-1,2-diaminoethane

: 284049-22-5
tert-butyl (2-isocyanatoethyl)carbamate

Guidance literature:: With sodium hydrogencarbonate; In dichloromethane; at 0 ℃; for 1h;

Reference yield:

: 39501-21-8
(2-azidocarbonyl-ethyl)-carbamic acid tert-butyl ester

: 284049-22-5
tert-butyl (2-isocyanatoethyl)carbamate

Guidance literature:: In toluene; at 65 ℃; for 0.166667h;
DOI:10.1021/jo990092e

Reference yield:

: C₁₁H₁₉NO₆

: 284049-22-5
tert-butyl (2-isocyanatoethyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: NaN₃ / tetrahydrofuran; H₂O / 0.08 h / -5 °C

2: toluene / 0.17 h / 65 °C

With sodium azide; In tetrahydrofuran; water; toluene; 1: Substitution / 2: Curtius rearrangement;
DOI:10.1021/jo990092e