methyl cis-4-[4-(5-cyclopentylamino[1.3.4]thiadiazol-2-ylcarbamoyl)-phenoxy]cyclohexanecarboxylate

Base Information

Chemical Name:methyl cis-4-[4-(5-cyclopentylamino[1.3.4]thiadiazol-2-ylcarbamoyl)-phenoxy]cyclohexanecarboxylate
CAS No.:1239311-38-6
Molecular Formula:C₂₂H₂₈N₄O₄S
Molecular Weight:444.555
Hs Code.:

Synonyms:methyl cis-4-[4-(5-cyclopentylamino[1.3.4]thiadiazol-2-ylcarbamoyl)-phenoxy]cyclohexanecarboxylate

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Chemical Property of methyl cis-4-[4-(5-cyclopentylamino[1.3.4]thiadiazol-2-ylcarbamoyl)-phenoxy]cyclohexanecarboxylate

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Technology Process of methyl cis-4-[4-(5-cyclopentylamino[1.3.4]thiadiazol-2-ylcarbamoyl)-phenoxy]cyclohexanecarboxylate

There total 6 articles about methyl cis-4-[4-(5-cyclopentylamino[1.3.4]thiadiazol-2-ylcarbamoyl)-phenoxy]cyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 941867-31-8
N-cyclopentyl[1.3.4]thiadiazole-2,5-diamine

: 1239311-09-1
methyl cis-4-(4-chlorocarbonylphenoxy)cyclohexanecarboxylate

: 1239311-38-6
methyl cis-4-[4-(5-cyclopentylamino[1.3.4]thiadiazol-2-ylcarbamoyl)-phenoxy]cyclohexanecarboxylate

Guidance literature:: With pyridine; In acetonitrile; for 72h; Inert atmosphere;

Reference yield:

: 25804-49-3
tert-butyl 4-hydroxybenzoate

: 1239311-38-6
methyl cis-4-[4-(5-cyclopentylamino[1.3.4]thiadiazol-2-ylcarbamoyl)-phenoxy]cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 18 h / 20 °C

2: trifluoroacetic acid / dichloromethane; diethyl ether / 5 h / 4 - 20 °C

3: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

4: pyridine / acetonitrile / 72 h / Inert atmosphere

With pyridine; oxalyl dichloride; di-isopropyl azodicarboxylate; N,N-dimethyl-formamide; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; acetonitrile;

Reference yield:

: 3618-03-9,17449-76-2,6125-57-1
trans-4-hydroxycyclohexane-1-carboxylic acid methyl ester

: 1239311-38-6
methyl cis-4-[4-(5-cyclopentylamino[1.3.4]thiadiazol-2-ylcarbamoyl)-phenoxy]cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 18 h / 20 °C

2: trifluoroacetic acid / dichloromethane; diethyl ether / 5 h / 4 - 20 °C

3: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

4: pyridine / acetonitrile / 72 h / Inert atmosphere

With pyridine; oxalyl dichloride; di-isopropyl azodicarboxylate; N,N-dimethyl-formamide; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; acetonitrile;