.beta.-D-Glucopyranoside, methyl 2-deoxy-2-1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethylamino-1-thio-

Base Information

Chemical Name:.beta.-D-Glucopyranoside, methyl 2-deoxy-2-1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethylamino-1-thio-
CAS No.:282526-14-1
Molecular Formula:C17H27 N O6 S
Molecular Weight:373.47
Hs Code.:

Synonyms:.beta.-D-Glucopyranoside, methyl 2-deoxy-2-1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethylamino-1-thio-

Suppliers and Price of .beta.-D-Glucopyranoside, methyl 2-deoxy-2-1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethylamino-1-thio-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of .beta.-D-Glucopyranoside, methyl 2-deoxy-2-1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethylamino-1-thio-

Chemical Property:

PSA：141.39000
LogP:0.36970

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of .beta.-D-Glucopyranoside, methyl 2-deoxy-2-1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethylamino-1-thio-

There total 11 articles about .beta.-D-Glucopyranoside, methyl 2-deoxy-2-1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethylamino-1-thio- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 212394-19-9
methyl 3,4,6-tri-O-acetyl-2-deoxy-2-N-[1-(4,4-dimethyl-2,6-dioxocyclohex-1-ylidene)ethyl]amino-1-thio-β-D-glucopyranoside

: 282526-14-1
methyl 2-deoxy-2-N-[1-(4,4-dimethyl-2,6-dioxocyclohex-1-ylidene)ethyl]amino-1-thio-β-D-glucopyranoside

Guidance literature:: With sodium methylate; In methanol; at 20 ℃;
DOI:10.1080/07328300500388685

Reference yield: 89.0%

: Acetic acid (2R,3S,4R,5R,6S)-3-acetoxy-2-acetoxymethyl-6-acetylsulfanyl-5-[1-(4,4-dimethyl-2,6-dioxo-cyclohexylidene)-ethylamino]-tetrahydro-pyran-4-yl ester

: 74-88-4
methyl iodide

: 282526-14-1
methyl 2-deoxy-2-N-[1-(4,4-dimethyl-2,6-dioxocyclohex-1-ylidene)ethyl]amino-1-thio-β-D-glucopyranoside

Guidance literature:: Acetic acid (2R,3S,4R,5R,6S)-3-acetoxy-2-acetoxymethyl-6-acetylsulfanyl-5-[1-(4,4-dimethyl-2,6-dioxo-cyclohexylidene)-ethylamino]-tetrahydro-pyran-4-yl ester; With sodium methylate; In methanol; at 20 ℃; for 0.666667h;

methyl iodide; In methanol; at 20 ℃; for 1h; Further stages.;
DOI:10.1021/jo010210+