(Z)-2,2'-(1-phenylprop-1-ene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

Base Information

Chemical Name:(Z)-2,2'-(1-phenylprop-1-ene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)
CAS No.:197251-03-9
Molecular Formula:C₂₁H₃₂B₂O₄
Molecular Weight:370.105
Hs Code.:

Synonyms:(Z)-2,2'-(1-phenylprop-1-ene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

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Chemical Property of (Z)-2,2'-(1-phenylprop-1-ene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

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Technology Process of (Z)-2,2'-(1-phenylprop-1-ene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

There total 2 articles about (Z)-2,2'-(1-phenylprop-1-ene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 673-32-5
1-Phenylprop-1-yne

: 73183-34-3
bis(pinacol)diborane

: 197251-03-9
(Z)-2,2'-(1-phenylprop-1-ene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

Guidance literature:: With methanol; potassium carbonate; In diethyl ether; at 40 ℃; for 12h; chemoselective reaction; Inert atmosphere;
DOI:10.1007/s11426-018-9344-4

Reference yield: 72.0%

: 673-32-5
1-Phenylprop-1-yne

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 121-43-7,63156-11-6
Trimethyl borate

: 197251-03-9
(Z)-2,2'-(1-phenylprop-1-ene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

Guidance literature:: 1-Phenylprop-1-yne; Trimethyl borate; With sodium; In tetrahydrofuran; mineral oil; at 20 ℃; for 0.5h; Schlenk technique; Inert atmosphere;

2,3-dimethyl-2,3-butane diol; In tetrahydrofuran; mineral oil; at 20 ℃; for 0.5h; Schlenk technique; Inert atmosphere;
DOI:10.1246/BCSJ.20200110

Reference yield: 80.0%

: 197251-03-9
(Z)-2,2'-(1-phenylprop-1-ene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

: 189999-35-7
[1,1'-biphenyl]-2,2'-iodonium trifluoromethanesulfonate

: 33498-62-3
9-methyl-10-phenylphenanthrene

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; sodium hydrogencarbonate; In tetrahydrofuran; water; for 16h; Inert atmosphere;
DOI:10.1007/s11426-018-9344-4