C₃₇H₄₈N₆O₈S

Base Information

Chemical Name:C₃₇H₄₈N₆O₈S
CAS No.:1610955-24-2
Molecular Formula:C₃₇H₄₈N₆O₈S
Molecular Weight:736.89
Hs Code.:

C<sub>37</sub>H<sub>48</sub>N<sub>6</sub>O<sub>8</sub>S

Synonyms:C₃₇H₄₈N₆O₈S

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Chemical Property of C₃₇H₄₈N₆O₈S

Chemical Property:

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Technology Process of C₃₇H₄₈N₆O₈S

There total 13 articles about C₃₇H₄₈N₆O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1610955-20-8
(2S,3S,4R,5S,6R)-2-(3-(4-(3-(2H-tetrazol-5-yl)propyl)benzyl)-4-methylphenyl)-6-(methylthio)tetrahydro-2H-pyran-3,4,5-triyl triacetate

: 40340-73-6
1-(chloroacetyl)-4-methylpiperazine

: 1610955-22-0
C₃₇H₄₈N₆O₈S

: 1610955-24-2
C₃₇H₄₈N₆O₈S

Guidance literature:: With triethylamine; In acetonitrile; at 60 ℃; for 18h;

Reference yield:

: 79669-49-1
5-bromo-2-methylbenzoic acid

: 1610955-22-0
C₃₇H₄₈N₆O₈S

: 1610955-24-2
C₃₇H₄₈N₆O₈S

Guidance literature:: Multi-step reaction with 13 steps

1.1: oxalyl dichloride; dmap / dichloromethane / 20 °C

2.1: triethylamine / dichloromethane / 0 - 20 °C

3.1: tetrahydrofuran / 2 h / 20 °C

4.1: triethylsilane; boron trifluoride diethyl etherate / acetonitrile / 2 h / 0 - 60 °C

5.1: tert-butylmagnesium chloride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

5.2: 1.5 h / -78 - 60 °C

6.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate; methanol; water; sodium hydroxide / 0.25 h

7.1: water; acetic acid / 7 h / 100 °C

8.1: dmap; triethylamine / acetonitrile / 1 h / 20 °C

9.1: thiourea; trimethylsilyl trifluoromethanesulfonate / 1,4-dioxane / 3 h / 80 °C

9.2: 18 h / 20 °C

10.1: tri tert-butylphosphoniumtetrafluoroborate; N-Methyldicyclohexylamine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1-methyl-pyrrolidin-2-one / 0.33 h / 160 °C / Microwave irradiation

11.1: palladium 10% on activated carbon; hydrogen / methanol / 5 h / 2068.65 Torr

12.1: trimethylsilylazide; di(n-butyl)tin oxide / toluene / 18 h / 90 °C

13.1: triethylamine / acetonitrile / 18 h / 60 °C

With methanol; triethylsilane; dmap; sodium tetrahydroborate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; oxalyl dichloride; trimethylsilyl trifluoromethanesulfonate; cerium(III) chloride heptahydrate; trimethylsilylazide; N-Methyldicyclohexylamine; palladium 10% on activated carbon; boron trifluoride diethyl etherate; tert-butylmagnesium chloride; water; hydrogen; di(n-butyl)tin oxide; acetic acid; triethylamine; thiourea; sodium hydroxide; tri tert-butylphosphoniumtetrafluoroborate; In tetrahydrofuran; 1,4-dioxane; 1-methyl-pyrrolidin-2-one; methanol; dichloromethane; toluene; acetonitrile;

Reference yield:

: 1500921-65-2
(5-bromo-2-methylphenyl)(4-chlorophenyl)methanone

: 1610955-22-0
C₃₇H₄₈N₆O₈S

: 1610955-24-2
C₃₇H₄₈N₆O₈S

Guidance literature:: Multi-step reaction with 10 steps

1.1: triethylsilane; boron trifluoride diethyl etherate / acetonitrile / 2 h / 0 - 60 °C

2.1: tert-butylmagnesium chloride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

2.2: 1.5 h / -78 - 60 °C

3.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate; methanol; water; sodium hydroxide / 0.25 h

4.1: water; acetic acid / 7 h / 100 °C

5.1: dmap; triethylamine / acetonitrile / 1 h / 20 °C

6.1: thiourea; trimethylsilyl trifluoromethanesulfonate / 1,4-dioxane / 3 h / 80 °C

6.2: 18 h / 20 °C

7.1: tri tert-butylphosphoniumtetrafluoroborate; N-Methyldicyclohexylamine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1-methyl-pyrrolidin-2-one / 0.33 h / 160 °C / Microwave irradiation

8.1: palladium 10% on activated carbon; hydrogen / methanol / 5 h / 2068.65 Torr

9.1: trimethylsilylazide; di(n-butyl)tin oxide / toluene / 18 h / 90 °C

10.1: triethylamine / acetonitrile / 18 h / 60 °C

With methanol; triethylsilane; dmap; sodium tetrahydroborate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; trimethylsilyl trifluoromethanesulfonate; cerium(III) chloride heptahydrate; trimethylsilylazide; N-Methyldicyclohexylamine; palladium 10% on activated carbon; boron trifluoride diethyl etherate; tert-butylmagnesium chloride; water; hydrogen; di(n-butyl)tin oxide; acetic acid; triethylamine; thiourea; sodium hydroxide; tri tert-butylphosphoniumtetrafluoroborate; In tetrahydrofuran; 1,4-dioxane; 1-methyl-pyrrolidin-2-one; methanol; toluene; acetonitrile;