2-Chlorobenzaldehyde oxime

Base Information

• Chemical Name: 2-Chlorobenzaldehyde oxime
• CAS No.: 3717-26-8
• Molecular Formula: C₇H₆ClNO
• Molecular Weight: 155.584
• European Community (EC) Number: 223-065-9
• UNII: 83D8ZJV2HS
• DSSTox Substance ID: DTXSID1063148
• Nikkaji Number: J1.249.462I
• Mol file: 3717-26-8.mol

Synonyms:2-Chlorobenzaldehyde oxime;3717-28-0;o-Chlorobenzaldoxime;Benzaldehyde, 2-chloro-, oxime;(E)-2-chlorobenzaldehyde oxime;2-Chlorobenzaldoxime;o-Chlorobenzaldehyde oxime;Benzaldehyde, o-chloro-, oxime;EINECS 223-065-9;NSC 61415;3717-26-8;AI3-07280;NSC-61415;2-chloro-benzaldehydeoxime;(E)-1-(2-chlorophenyl)-N-hydroxymethanimine;83D8ZJV2HS;(NE)-N-[(2-chlorophenyl)methylidene]hydroxylamine;SCHEMBL534274;(Z)-2-Chlorobenzaldehydeoxime;2-chlorobenzenecarbaldehyde oxime;DTXSID1063148;2-Chlorobenzaldehyde oxime, 98%;HMS1783G02;STR07747;[C(E)]-2-Chlorobenzaldehyde oxime;MFCD00016406;STK045175;AKOS000304459;AKOS025311003;Benzaldehyde, o-chloro-, oxime, (E)-;Benzaldehyde, 2-chloro-, oxime, (E)-;NCGC00323570-01;11L-339S;Benzaldehyde, 2-chloro-, oxime, [C(E)]-;CS-0320198;AB01319049-02;A823548;Z49568320;(E)-N-[(2-CHLOROPHENYL)METHYLIDENE]HYDROXYLAMINE

Chemical Property of 2-Chlorobenzaldehyde oxime

Chemical Property:

• PSA: 32.59000
• LogP: 2.14810
• XLogP3: 2.6
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 155.0137915
• Heavy Atom Count: 10
• Complexity: 127

Purity/Quality:

2-Chlorobenzaldehyde oxime ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C(=C1)C=NO)Cl
• Isomeric SMILES: C1=CC=C(C(=C1)/C=N/O)Cl

Technology Process of 2-Chlorobenzaldehyde oxime

There total 16 articles about 2-Chlorobenzaldehyde oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2-chloro-benzaldehyde (89-98-5) → 2-chlorobenzaldoxime (3717-26-8,3717-27-9,3717-28-0)

Guidance literature:

With hydroxylamine hydrochloride; zinc(II) oxide; at 80 ℃; for 0.0833333h;

DOI:10.1055/s-2002-31964

Reference yield: 95.0%

ethyl methyl ketone oxime (96-29-7) + 2-chloro-benzaldehyde (89-98-5) → (E)-2-chlorobenzaldehyde oxime (3717-26-8,3717-27-9,3717-28-0)

Guidance literature:

With perchloric acid; In water; at 23 ℃; for 24h; Reagent/catalyst; Inert atmosphere; Green chemistry;

DOI:10.1039/c6gc02156e

Reference yield: 92.0%

2-chloro-benzaldehyde (89-98-5) → (E)-2-chlorobenzaldehyde oxime (3717-26-8,3717-27-9,3717-28-0)

Guidance literature:

With hydroxylamine hydrochloride; potassium carbonate; In ethanol; water; at 60 ℃; for 0.0666667h; pH=10; Sonication;

upstream raw materials:

(E)-2-chlorobenzaldehyde oxime

benzene

hydrogenchloride

2-chloro-benzaldehyde

Downstream raw materials:

2-chloro-N-hydroxybenzimidoyl chloride

2-Chlorobenzonitrile

2-chlorobenzamide

2-chloro-benzaldehyde