2,5,8-tris(diphenylamino)-1,3,4,6,7,9,9b-heptaazaphenalene

Base Information

• Chemical Name: 2,5,8-tris(diphenylamino)-1,3,4,6,7,9,9b-heptaazaphenalene
• CAS No.: 106407-81-2
• Molecular Formula: C₄₂H₃₀N₁₀
• Molecular Weight: 674.767
• Mol file: 106407-81-2.mol

Synonyms:2,5,8-tris(diphenylamino)-1,3,4,6,7,9,9b-heptaazaphenalene

Chemical Property of 2,5,8-tris(diphenylamino)-1,3,4,6,7,9,9b-heptaazaphenalene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,5,8-tris(diphenylamino)-1,3,4,6,7,9,9b-heptaazaphenalene

There total 3 articles about 2,5,8-tris(diphenylamino)-1,3,4,6,7,9,9b-heptaazaphenalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene (6710-92-5) + diphenylamine (122-39-4) → 2,5,8-tris(diphenylamino)-1,3,4,6,7,9,9b-heptaazaphenalene (106407-81-2)

Guidance literature:

In xylene; at 80 ℃; for 14h;

Reference yield:

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene (6710-92-5) + diphenylamine (122-39-4) + diethylamine (109-89-7) → 2,5,8-tris(diphenylamino)-1,3,4,6,7,9,9b-heptaazaphenalene (106407-81-2)

Guidance literature:

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene; diphenylamine; In para-xylene; at 20 ℃; Reflux;

diethylamine; In para-xylene; for 1h; Reflux;

DOI:10.1039/c0nj00989j

Reference yield:

→ 2,5,8-tris(diphenylamino)-1,3,4,6,7,9,9b-heptaazaphenalene (106407-81-2)

Guidance literature:

Cyamelurchlorid(I),Diphenylamin i.Xylol;

upstream raw materials:

2,5,8-trichloro-1,3,4,6,7,9,9b-heptaazaphenalene

diphenylamine

diethylamine