Dibenzyl-[(S)-3-(tert-butyl-dimethyl-silanyloxy)-1-trityloxymethyl-propyl]-amine

Base Information

Chemical Name:Dibenzyl-[(S)-3-(tert-butyl-dimethyl-silanyloxy)-1-trityloxymethyl-propyl]-amine
CAS No.:214832-92-5
Molecular Formula:C₄₃H₅₁NO₂Si
Molecular Weight:641.969
Hs Code.:

Synonyms:Dibenzyl-[(S)-3-(tert-butyl-dimethyl-silanyloxy)-1-trityloxymethyl-propyl]-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dibenzyl-[(S)-3-(tert-butyl-dimethyl-silanyloxy)-1-trityloxymethyl-propyl]-amine

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Technology Process of Dibenzyl-[(S)-3-(tert-butyl-dimethyl-silanyloxy)-1-trityloxymethyl-propyl]-amine

There total 2 articles about Dibenzyl-[(S)-3-(tert-butyl-dimethyl-silanyloxy)-1-trityloxymethyl-propyl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 76-83-5
trityl chloride

: 152299-13-3
(2S)-4-{[tert-butyl(dimethyl)silyl]oxy}-2-(dibenzylamino)butan-1-ol

: 214832-92-5
Dibenzyl-[(S)-3-(tert-butyl-dimethyl-silanyloxy)-1-trityloxymethyl-propyl]-amine

Guidance literature:: With dmap; triethylamine; In dichloromethane; for 14h; Ambient temperature;
DOI:10.1055/s-1998-6100

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 214832-92-5
Dibenzyl-[(S)-3-(tert-butyl-dimethyl-silanyloxy)-1-trityloxymethyl-propyl]-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / Et₃N, DMAP / CH₂Cl₂ / 8 h / 40 °C

2: 91 percent / Et₃N, DMAP / CH₂Cl₂ / 14 h / Ambient temperature

With dmap; triethylamine; In dichloromethane;
DOI:10.1055/s-1998-6100

Reference yield: 82.0%

: 214832-92-5
Dibenzyl-[(S)-3-(tert-butyl-dimethyl-silanyloxy)-1-trityloxymethyl-propyl]-amine

: 214832-94-7
(S)-3-Dibenzylamino-4-trityloxy-butan-1-ol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; diethyl ether; for 14h; Ambient temperature;
DOI:10.1055/s-1998-6100