2-amino-1-benzoylnaphthalene

Base Information

• Chemical Name: 2-amino-1-benzoylnaphthalene
• CAS No.: 116400-82-9
• Molecular Formula: C₁₇H₁₃NO
• Molecular Weight: 247.296
• Mol file: 116400-82-9.mol

Synonyms:2-amino-1-benzoylnaphthalene

Chemical Property of 2-amino-1-benzoylnaphthalene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 2-amino-1-benzoylnaphthalene

There total 7 articles about 2-amino-1-benzoylnaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2-chloro-[1]naphthyl)-phenyl ketone → 2-amino-1-benzoylnaphthalene (116400-82-9)

Guidance literature:

With ammonium hydroxide; copper; at 230 ℃; under 51485.6 Torr;

Reference yield:

2-aminonaphthalene-1-carbonitrile (7066-13-9) + phenylmagnesium bromide → 2-amino-1-benzoylnaphthalene (116400-82-9)

Guidance literature:

With hydrogenchloride; Yield given. Multistep reaction; 1.) Et₂O, reflux, 1 h, 2.) Et₂O, 30 deg C, 5 h;

DOI:10.1021/jm00032a007

Reference yield:

2-nitronaphthalene (581-89-5) → 2-amino-1-benzoylnaphthalene (116400-82-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) potassium cyanide, potassium hydroxide, 2.) 5percent NaOH / 1.) DMF, 50 deg C, 36 h, 2.) reflux

2: 2.) 2N HCl / 1.) ether, reflux, 2.) reflux

With hydrogenchloride; potassium cyanide; potassium hydroxide; sodium hydroxide;

upstream raw materials:

N-(1-benzoyl-[2]naphthyl)-benzamide

2-aminonaphthalene-1-carbonitrile

phenylmagnesium bromide

2-nitronaphthalene

Downstream raw materials:

1-phenyl-benzo[f]quinolin-3-ol

N-(1-benzoyl-[2]naphthyl)-acetamide

2--1-benzoylnaphthalene

5-phenyl-1,3-dihydronaphtho<2,1-e><1,4>diazepin-2-one