2-cyano-N'-[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]acetohydrazide

Base Information

• Chemical Name: 2-cyano-N'-[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]acetohydrazide
• CAS No.: 1297309-96-6
• Molecular Formula: C₁₅H₁₅N₅O
• Molecular Weight: 281.317

Synonyms:2-cyano-N'-[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]acetohydrazide

Chemical Property of 2-cyano-N'-[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]acetohydrazide

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Technology Process of 2-cyano-N'-[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]acetohydrazide

There total 1 articles about 2-cyano-N'-[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]acetohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

Cyanoacetohydrazide (140-87-4) + methyl 5-methyl-2-phenyl-4-imidazolyl ketone (28824-91-1) → 2-cyano-N'-[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]acetohydrazide (1297309-96-6)

Guidance literature:

In ethanol; for 1h; Reflux;

DOI:10.1016/j.ejmech.2011.01.062

Reference yield: 76.0%

2-cyano-N'-[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]acetohydrazide (1297309-96-6) + 3-(1-benzofuran-2-yl)-1-phenyl-1H-pyrazole-4-carbaldehyde (372098-13-0) → 3-[3-(benzofuran-2-yl)-1-phenyl-1H-pyrazol-4-yl]-2-cyano-N'-[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]acrylohydrazide (1297310-02-1)

Guidance literature:

With piperidine; In ethanol; for 3h; Reflux;

DOI:10.1016/j.ejmech.2011.01.062

Reference yield: 73.0%

2-cyano-N'-[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]acetohydrazide (1297309-96-6) + 1-phenyl-3-thiophen-2-yl-1H-pyrazole-4-carbaldehyde (210825-11-9) → 2-cyano-N'-[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]-3-[1-phenyl-3-(thiophen-2-yl)-1H-pyrazol-4-yl]acrylohydrazide (1297310-00-9)

Guidance literature:

With piperidine; In ethanol; for 3h; Reflux;

DOI:10.1016/j.ejmech.2011.01.062

upstream raw materials:

Cyanoacetohydrazide

methyl 5-methyl-2-phenyl-4-imidazolyl ketone

Downstream raw materials:

2-cyano-N'-[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]-3-[1-phenyl-3-(thiophen-2-yl)-1H-pyrazol-4-yl]acrylohydrazide

7-hydroxy-2-imino-N'-[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]-2H-chromene-3-carbohydrazide

3-[3-(benzofuran-2-yl)-1-phenyl-1H-pyrazol-4-yl]-2-cyano-N'-[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]acrylohydrazide

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