carbonic acid [1-(2-benzyloxy-1-methylethyl)-2,4,4-trimethyl-3,5-dioxopentyl ester] 2,2,2-trichloroethyl ester

Base Information

Chemical Name:carbonic acid [1-(2-benzyloxy-1-methylethyl)-2,4,4-trimethyl-3,5-dioxopentyl ester] 2,2,2-trichloroethyl ester
CAS No.:637003-51-1
Molecular Formula:C₂₁H₂₇Cl₃O₆
Molecular Weight:481.801
Hs Code.:

Synonyms:carbonic acid [1-(2-benzyloxy-1-methylethyl)-2,4,4-trimethyl-3,5-dioxopentyl ester] 2,2,2-trichloroethyl ester

Suppliers and Price of carbonic acid [1-(2-benzyloxy-1-methylethyl)-2,4,4-trimethyl-3,5-dioxopentyl ester] 2,2,2-trichloroethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of carbonic acid [1-(2-benzyloxy-1-methylethyl)-2,4,4-trimethyl-3,5-dioxopentyl ester] 2,2,2-trichloroethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of carbonic acid [1-(2-benzyloxy-1-methylethyl)-2,4,4-trimethyl-3,5-dioxopentyl ester] 2,2,2-trichloroethyl ester

There total 2 articles about carbonic acid [1-(2-benzyloxy-1-methylethyl)-2,4,4-trimethyl-3,5-dioxopentyl ester] 2,2,2-trichloroethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 666739-81-7
carbonic acid [1-(2-benzyloxy-1-methylethyl)-5,5-diisopropoxy-2,4,4-trimethyl-3-oxopentyl ester] 2,2,2-trichloroethyl ester

: 637003-51-1
carbonic acid [1-(2-benzyloxy-1-methylethyl)-2,4,4-trimethyl-3,5-dioxopentyl ester] 2,2,2-trichloroethyl ester

Guidance literature:: With toluene-4-sulfonic acid; In tetrahydrofuran; at 70 ℃; for 5h;
DOI:10.1021/ja046992g

Reference yield:

: 503818-15-3
7-benzyloxy-5-hydroxy-1,1-diisopropyl-2,2,4,6-tetramethylheptan-3-one

: 637003-51-1
carbonic acid [1-(2-benzyloxy-1-methylethyl)-2,4,4-trimethyl-3,5-dioxopentyl ester] 2,2,2-trichloroethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / pyridine / CH₂Cl₂ / 1 h / 20 °C

2: 76 percent / aq. p-TsOH / tetrahydrofuran / 5 h / 70 °C

With pyridine; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja046992g

Reference yield: 80.0%

: 540-88-5
acetic acid tert-butyl ester

: 637003-51-1
carbonic acid [1-(2-benzyloxy-1-methylethyl)-2,4,4-trimethyl-3,5-dioxopentyl ester] 2,2,2-trichloroethyl ester

: C₂₇H₃₉Cl₃O₈

Guidance literature:: acetic acid tert-butyl ester; With lithium diisopropyl amide; In diethyl ether; at -78 ℃; for 0.5h;

carbonic acid [1-(2-benzyloxy-1-methylethyl)-2,4,4-trimethyl-3,5-dioxopentyl ester] 2,2,2-trichloroethyl ester; In diethyl ether; at -78 ℃; for 1.5h;