pyridine-2-carboxaldehyde-4-chlorobenzoylhydrazone

Base Information

Chemical Name:pyridine-2-carboxaldehyde-4-chlorobenzoylhydrazone
CAS No.:119259-99-3
Molecular Formula:C₁₃H₁₀ClN₃O
Molecular Weight:259.695
Hs Code.:

Synonyms:pyridine-2-carboxaldehyde-4-chlorobenzoylhydrazone

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Chemical Property of pyridine-2-carboxaldehyde-4-chlorobenzoylhydrazone

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Technology Process of pyridine-2-carboxaldehyde-4-chlorobenzoylhydrazone

There total 1 articles about pyridine-2-carboxaldehyde-4-chlorobenzoylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1121-60-4
pyridine-2-carbaldehyde

: 536-40-3
4-chlorobenzoic acid hydrazide

: 119259-99-3
pyridine-2-carboxaldehyde-4-chlorobenzoylhydrazone

Guidance literature:: With hydrogenchloride; In ethanol; Heating;
DOI:10.1002/1521-3773(20021104)41:21<4096::AID-ANIE4096>3.0.CO;2-0

Reference yield: 95.0%

: lanthanum(III) nitrate hexahydrate

: 119259-99-3
pyridine-2-carboxaldehyde-4-chlorobenzoylhydrazone

: 841232-93-7
[La(NO₃)3(pyridine-2-carboxaldehyde-4-chlorobenzoylhydrazone)2]

Guidance literature:: In methanol; byproducts: H2O; prepn. in dry box under N2 atm.; soln. of org. ligand in MeOH added to soln. of lanthanide nitrate hydrate in MeOH; soln. stirred for 10-20 min at room temp.; filtered; washed (MeOH); dried (vac., anhyd. CaCl2); elem. anal.;
DOI:10.1081/SIM-200026268

Reference yield: 93.0%

: cerium(III) nitrate hexahydrate

: 119259-99-3
pyridine-2-carboxaldehyde-4-chlorobenzoylhydrazone

: 841232-94-8
[Ce(NO₃)3(pyridine-2-carboxaldehyde-4-chlorobenzoylhydrazone)2]

Guidance literature:: In methanol; byproducts: H2O; prepn. in dry box under N2 atm.; soln. of org. ligand in MeOH added to soln. of lanthanide nitrate hydrate in MeOH; soln. stirred for 10-20 min at room temp.; filtered; washed (MeOH); dried (vac., anhyd. CaCl2); elem. anal.;
DOI:10.1081/SIM-200026268