10-(4-(5-(9,9-dihexyl-7-(5'-(pyridin-4-yl)-2,2'-bithiophen-5-yl)-9H-fluoren-2-yl)thiophen-2-yl)phenoxy)decan-1-ol

Base Information

Chemical Name:10-(4-(5-(9,9-dihexyl-7-(5'-(pyridin-4-yl)-2,2'-bithiophen-5-yl)-9H-fluoren-2-yl)thiophen-2-yl)phenoxy)decan-1-ol
CAS No.:1263559-53-0
Molecular Formula:C₅₈H₆₇NO₂S₃
Molecular Weight:906.373
Hs Code.:

Synonyms:10-(4-(5-(9,9-dihexyl-7-(5'-(pyridin-4-yl)-2,2'-bithiophen-5-yl)-9H-fluoren-2-yl)thiophen-2-yl)phenoxy)decan-1-ol

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Chemical Property of 10-(4-(5-(9,9-dihexyl-7-(5'-(pyridin-4-yl)-2,2'-bithiophen-5-yl)-9H-fluoren-2-yl)thiophen-2-yl)phenoxy)decan-1-ol

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Technology Process of 10-(4-(5-(9,9-dihexyl-7-(5'-(pyridin-4-yl)-2,2'-bithiophen-5-yl)-9H-fluoren-2-yl)thiophen-2-yl)phenoxy)decan-1-ol

There total 10 articles about 10-(4-(5-(9,9-dihexyl-7-(5'-(pyridin-4-yl)-2,2'-bithiophen-5-yl)-9H-fluoren-2-yl)thiophen-2-yl)phenoxy)decan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1263559-50-7
4-(5'-(7-(5-(4-(10-(tert-butyldimethylsilyloxy)decyloxy)phenyl)thiophen-2-yl)-9,9-dihexyl-9H-fluoren-2-yl)-2,2'-bithiophen-5-yl)pyridine

: 1263559-53-0
10-(4-(5-(9,9-dihexyl-7-(5'-(pyridin-4-yl)-2,2'-bithiophen-5-yl)-9H-fluoren-2-yl)thiophen-2-yl)phenoxy)decan-1-ol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; hexane; at 20 ℃; for 12.1667h; Cooling with ice;
DOI:10.1016/j.polymer.2010.10.018

Reference yield:

: 2-{4-[10-(tert-butyl-dimethyl-silanyloxy)-decyl]-phenyl}-4,4,5,5-tetramethyl-[1,3,2] dioxaborolane

: 1263559-53-0
10-(4-(5-(9,9-dihexyl-7-(5'-(pyridin-4-yl)-2,2'-bithiophen-5-yl)-9H-fluoren-2-yl)thiophen-2-yl)phenoxy)decan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / ethanol; toluene / Reflux

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / ethanol; toluene / 24 h / Reflux; Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran; hexane / 12.17 h / 20 °C / Cooling with ice

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; potassium carbonate; In tetrahydrofuran; ethanol; hexane; toluene; 1: Suzuki coupling;
DOI:10.1016/j.polymer.2010.10.018

Reference yield:

: 1263559-47-2
(10-(4-(5-(7-(5-bromothiophen-2-yl)-9,9-dihexyl-9H-fluoren-2-yl)thiophen-2-yl)phenoxy)decyloxy) (tert-butyl)dimethylsilane

: 1263559-53-0
10-(4-(5-(9,9-dihexyl-7-(5'-(pyridin-4-yl)-2,2'-bithiophen-5-yl)-9H-fluoren-2-yl)thiophen-2-yl)phenoxy)decan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / ethanol; toluene / 24 h / Reflux; Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran; hexane / 12.17 h / 20 °C / Cooling with ice

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; potassium carbonate; In tetrahydrofuran; ethanol; hexane; toluene;
DOI:10.1016/j.polymer.2010.10.018