N-<<<(tyrosylglycyl)amino>methyl>hydroxyphosphinyl>phenylalanylleucine disodium salt

Base Information

Chemical Name:N-<<<(tyrosylglycyl)amino>methyl>hydroxyphosphinyl>phenylalanylleucine disodium salt
CAS No.:96914-93-1
Molecular Formula:C₂₇H₃₆N₅O₈P*2Na
Molecular Weight:635.565
Hs Code.:

Synonyms:N-<<<(tyrosylglycyl)amino>methyl>hydroxyphosphinyl>phenylalanylleucine disodium salt

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Chemical Property of N-<<<(tyrosylglycyl)amino>methyl>hydroxyphosphinyl>phenylalanylleucine disodium salt

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Technology Process of N-<<<(tyrosylglycyl)amino>methyl>hydroxyphosphinyl>phenylalanylleucine disodium salt

There total 7 articles about N-<<<(tyrosylglycyl)amino>methyl>hydroxyphosphinyl>phenylalanylleucine disodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 96914-85-1
C₅₆H₆₂N₅O₁₀P

: 96914-93-1
N-<<<(tyrosylglycyl)amino>methyl>hydroxyphosphinyl>phenylalanylleucine disodium salt

Guidance literature:: With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In ethanol; water; for 6h; under 760 Torr;
DOI:10.1021/jm00147a015

Reference yield:

: 16677-35-3
N-benzyloxycarbonyl-O-benzyl-(S)tyrosyl-glycine methyl ester

: 96914-93-1
N-<<<(tyrosylglycyl)amino>methyl>hydroxyphosphinyl>phenylalanylleucine disodium salt

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / 0.25N NaOH / acetonitrile / 1.5 h / Ambient temperature

2: 11 percent / HOBt, DCC / tetrahydrofuran / 36 h / Ambient temperature

3: 92 percent / H₂, NaHCO₃ / 10percent Pd/C / ethanol; H₂O / 6 h / 760 Torr

With sodium hydroxide; hydrogen; sodium hydrogencarbonate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; ethanol; water; acetonitrile;
DOI:10.1021/jm00147a015

Reference yield:

: 51952-34-2
(S)-2-(2-(((benzyloxy)carbonyl)amino)-3-(4-(benzyloxy)phenyl)propanamido)acetic acid

: 96914-93-1
N-<<<(tyrosylglycyl)amino>methyl>hydroxyphosphinyl>phenylalanylleucine disodium salt

Guidance literature:: Multi-step reaction with 2 steps

1: 11 percent / HOBt, DCC / tetrahydrofuran / 36 h / Ambient temperature

2: 92 percent / H₂, NaHCO₃ / 10percent Pd/C / ethanol; H₂O / 6 h / 760 Torr

With hydrogen; sodium hydrogencarbonate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; ethanol; water;
DOI:10.1021/jm00147a015