methanesulfonic acid 3-(tert-butyl-dimethyl-silanyloxymethyl)-benzyl ester

Base Information

• Chemical Name: methanesulfonic acid 3-(tert-butyl-dimethyl-silanyloxymethyl)-benzyl ester
• CAS No.: 1006301-26-3
• Molecular Formula: C₁₅H₂₆O₄SSi
• Molecular Weight: 330.521

Synonyms:methanesulfonic acid 3-(tert-butyl-dimethyl-silanyloxymethyl)-benzyl ester

Chemical Property of methanesulfonic acid 3-(tert-butyl-dimethyl-silanyloxymethyl)-benzyl ester

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Technology Process of methanesulfonic acid 3-(tert-butyl-dimethyl-silanyloxymethyl)-benzyl ester

There total 1 articles about methanesulfonic acid 3-(tert-butyl-dimethyl-silanyloxymethyl)-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanesulfonyl chloride (124-63-0) + 3-(tert-Butyldimethylsiloxymethyl)benzyl Alcohol (81805-53-0) → methanesulfonic acid 3-(tert-butyl-dimethyl-silanyloxymethyl)-benzyl ester (1006301-26-3)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 ℃; for 0.75h;

Reference yield:

methanesulfonic acid 3-(tert-butyl-dimethyl-silanyloxymethyl)-benzyl ester (1006301-26-3) + tert-butyl (1R,3'S)-3'-[(cyclopropylamino)carbonyl]-5,6-difluoro-1'H,3H-spiro[2-benzofuran-1,4'-piperidine]-1'-carboxylate (1266727-97-2) → tert-butyl (cis-1,3')-3'-{[[3-({[tertbutyl(dimethyl)silyl]oxy}methyl)benzyl](cyclopropyl)amino]carbonyl}-5,6-difluoro-1'H,3Hspiro[2-benzofuran-1,4'-piperidine]-1'-carboxylate

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 6h;

Reference yield:

methanesulfonic acid 3-(tert-butyl-dimethyl-silanyloxymethyl)-benzyl ester (1006301-26-3) + sodium cyanide (143-33-9,25596-52-5) → [3-(tert-butyl-dimethyl-silanyloxymethyl)-phenyl]-acetonitrile (1006301-23-0)

Guidance literature:

In N,N-dimethyl-formamide; at 60 ℃; for 2h;

upstream raw materials:

methanesulfonyl chloride

3-(tert-Butyldimethylsiloxymethyl)benzyl Alcohol

Downstream raw materials:

[3-(tert-butyl-dimethyl-silanyloxymethyl)-phenyl]-acetonitrile

{1-[3-({[tert-butyl(dimethyl)silyl]oxy}methyl)benzyl]-6-methoxy-2-methyl-1H-indole-3-yl}(4-methylphenyl)methanone

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